Method for measuring sodium in sodium humate
A determination method, sodium humate technology, applied in the direction of material excitation analysis, thermal excitation analysis, etc., can solve the problems of high detection limit and low sensitivity, and achieve the effects of fast analysis speed, simple operation, high precision and accuracy
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[0021] Embodiment: a kind of assay method of sodium in sodium humate
[0022] Weigh 0.1000g (accurate to 0.0001g) of 3 kinds of humic acid samples into the digestive tube, add 5ml H 2 SO 4 , digested in a temperature-controlled far-infrared digestion furnace, first heated at 80-100°C, then raised the temperature, and added 30g / L H 2 o 2 10 drops, shake well, continue heating for 10 minutes, remove and cool for 2 minutes, add 30g / L H 2 o 2 Shake 10 drops, heat on a far-infrared digestion furnace for 10 minutes, repeat this process until the solution is clear, cool to room temperature, transfer to a 100ml volumetric flask with pure water, filter after constant volume; prepare Na standard solution, set ICP-AES instrument working parameters: RF power is 1150w, flushing pump speed is 100rpm, analysis pump speed is 50rpm, pump delay time is 5 seconds, atomizer gas flow is 0.70L / min, auxiliary gas flow is 0.50L / min, the sodium spectral line is 588.9nm, and the number of repetit...
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