Efficient deep dyeing promoter, and preparation and after treatment application methods thereof
An application method and a technology of a darkening agent, which are applied in the fields of fiber processing, textiles and papermaking, etc., can solve the problems of low darkening rate, unexplained darkening rate, and insufficient application effect, etc., so as to improve the darkening effect and fabric The apparent dark color effect is improved and the color difference is small
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Embodiment 1
[0051] 1) Preparation of pre-emulsion: mix 20 g of methyl methacrylate and 1 g of ethylene glycol diacrylate as the oil phase; add 1 g of cationic emulsifier 1831 and nonionic emulsifier Pingping O-15 (both The dosage ratio is 2:1), 0.2 g of glacial acetic acid, dissolved in 31 g of deionized water as the water phase. Mix the water phase and the oil phase, and stir at 1500 rpm for 35 minutes at room temperature to obtain a pre-emulsion;
[0052] 2) Prepare the primer: add 0.35 g of 1831 and Pingping O-15 (the ratio of the two is 1:1), 0.06 g of azobisisobutylimidazoline hydrochloride and 47 g of deionized water, at room temperature Stir to dissolve evenly. The primer is all packed into a four-necked flask connected with stirring, thermometer, condenser and nitrogen pipe;
[0053] 3) Polymerization reaction: Inflate nitrogen into the flask with primer for 20 minutes to remove oxygen, stir at the same time, heat up the water bath, and when the temperature in the flask is stabl...
Embodiment 2
[0055] Step 1) According to Example 1, the crosslinking agent used was changed to 2 g ethylene glycol dimethacrylate, and the deionized water was 29.8 g;
[0056] Steps 2) and 3) are the same as in Example 1. The measured solid content of the darkening agent was 21.9%, and the monomer conversion rate was 99.6%.
Embodiment 3
[0058] 1) Preparation of pre-emulsion: Mix 25 g of methyl methacrylate and 2.5 g of ethylene glycol dimethacrylate into the oil phase; add 1.1 g of cationic emulsifier 1227 and nonionic emulsifier Pingping O-15 ( The ratio of the two is 2:1), 0.25 g of glacial acetic acid, dissolved in 28 g of deionized water as the water phase. Mix the water phase and the oil phase, and stir at 1500 rpm for 35 minutes at room temperature to obtain a pre-emulsion;
[0059] 2) Prepare the primer: add 0.5 g of 1227 and Pingping O-15 (the ratio of the two is 1:1), 0.09 g of azobisisobutylimidazoline hydrochloride and 42.6 g of deionized water, at room temperature Stir to dissolve evenly. The primer is all packed into a four-necked flask connected with stirring, thermometer, condenser and nitrogen pipe;
[0060] 3) Polymerization reaction: Inflate nitrogen into the flask with primer for 20 minutes to remove oxygen, stir at the same time, heat up the water bath, and when the temperature in the fl...
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