A kind of automatic liquid-stopping nuclear pore filter membrane for precision infusion and its preparation method
A nuclear pore filter membrane, automatic technology, applied in the field of preparation of automatic liquid-stop nuclear pore filter membrane for precision infusion, can solve the problems of high filtration speed, ordinary polyester nuclear pore membrane cannot be used as a liquid medicine filter membrane, etc., to achieve the method simple effect
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Embodiment 1
[0032] A method for preparing a precision transfusion automatic liquid-stopping nuclear pore filter, comprising the following steps: using an accelerator to produce 16MeV / u Xe-132 particles to irradiate a polyester film with a thickness of 8 μm, at 55°C and 6.5mol / L Etching in aqueous sodium hydroxide solution for 60 minutes; cleaning in 60°C, 1mol / L sodium hydroxide aqueous solution for 10 minutes; then cleaning in deionized water; in 80°C modification solution, ultrasonic soaking for 10 minutes before stopping the ultrasonic Soak for 40 minutes, then continue ultrasonic soaking for 10 minutes; wash in deionized water; dry at 50°C to make a nuclear pore filter membrane for precision infusion with automatic liquid stop. The membrane has a pore size of 0.1 μm and a water contact angle of 30.0°. The thickness is 7.9 μm, and when used as a filter membrane for precision infusion filters, the liquid stop height can reach 3.0 meters.
[0033] The modifying solution is composed of 15...
Embodiment 2
[0035] A method for preparing a precision infusion automatic liquid-stop nuclear pore filter, comprising the following steps: a polyester film with a thickness of 12 μm irradiated with Kr-84 particles of 15 MeV / u produced by an accelerator is heated at 65°C and 7.0mol / L Etching in aqueous sodium hydroxide solution for 30 minutes; cleaning in 55°C, 1mol / L sodium hydroxide aqueous solution for 10 minutes; then cleaning in deionized water; in 70°C modified solution, ultrasonic soaking for 8 minutes, and then stop the ultrasonic Soak for 30 minutes, then continue ultrasonic soaking for 8 minutes; wash in deionized water; dry at 40°C to make a nuclear pore filter membrane for precision infusion with automatic liquid stop. The membrane has a pore size of 2.0 μm and a water contact angle of 25.3° 10μm, when used as a filter membrane for precision infusion filters, the liquid stop height can reach 3.0 meters.
[0036] The modifying liquid is composed of 20 parts of potassium dichromat...
Embodiment 3
[0038] A method for preparing an automatic liquid-stopping nuclear pore filter for precision infusion, characterized in that it comprises the following steps:
[0039]A polyester film with a thickness of 30 μm irradiated with 15 MeV / u Kr-84 particles generated by an accelerator is etched in 75°C, 7.0mol / L sodium hydroxide aqueous solution for 30 minutes; at 75°C, 0.5 / L sodium hydroxide Wash in aqueous solution for 10 minutes; then wash in deionized water; in 60°C modified solution, first soak in ultrasonic for 3 minutes, then stop ultrasonic soaking for 20 minutes, and continue ultrasonic soaking for 3 minutes; wash in deionized water; bake at 60°C After drying, it can be made into a nuclear pore filter membrane with automatic liquid stop for precision infusion. The membrane has a pore size of 5.0 μm, a water contact angle of 15.1°, and a thickness of 24 μm. When used as a filter membrane for precision infusion filters, the liquid stop height can reach 2.2 meters.
[0040] The...
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