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Wax-based blade coating patterning method

A patterned and patterned technology, applied in the field of micromachining, to achieve the effect of less sample injection, high stability and easy preparation

Inactive Publication Date: 2014-06-25
SOUTHEAST UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004]The traditional wax printing micromachining method still has low resolution, needs heating, and consumes a lot of samples. complex
Inkjet printing requires expensive or custom instrumentation and operator requirements
In addition to the complicated operation and low resolution, there is still a problem with the current microfluidic chips on paper that the flow rate is too slow. Traditional paper chips need 15-20 minutes to flow through a 5 cm long paper channel.

Method used

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  • Wax-based blade coating patterning method
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  • Wax-based blade coating patterning method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Example 1 The patterning method based on scraping on wax is used for photonic crystal patterning:

[0034] (1) Hydrophilic treatment of polypropylene plastic sheet (PP), using 1%-10% (w / w) Tween-20 aqueous solution, soaking in piranha solution or Plasma plasma treatment machine, etc.

[0035] (2) Use CorelDraw12 to design the pattern SEU (length 1.5 mm, width 0.6 mm), and use a wax jet printer to print the wax pattern on PP.

[0036] (3) Five different particle sizes (200, 240, 270, 288, 950 nm) of SiO 2 Photonic crystal colloid aqueous solution (mass fraction 40%) is applied on the printed PP with a scraper.

[0037] (4) The solvent evaporates naturally at room temperature, and SiO 2 The nanoparticles form photonic crystal patterns in the wax-free hollow areas. And have the characteristics of color change when viewed from different angles ( image 3 )

[0038] (5) Reflection spectrum characterization of the pattern ( Figure 4 ) and SEM characterization ( Figur...

Embodiment 2

[0039] Example 2 The patterning method based on scraping coating on wax is used to pattern cellulose to make a microfluidic chip:

[0040] (1) Hydrophilic treatment of PP surface with 1% (w / w) Tween-20 aqueous solution

[0041] (2) Use CorelDraw12 to design microfluidic patterns (the narrowest channel width is 50 μm), and use a wax jet printer to print the wax patterns on PP.

[0042] (3) Microcrystalline cellulose with small particle size was prepared by acidolysis of microcrystalline cellulose: 10 g of microcrystalline cellulose (particle size ~20 μm) was added to 10 mL of sulfuric acid (mass fraction 64%), mixed thoroughly Stir at high speed at 45 ℃ for 30 min, centrifuge and wash several times to make the suspension pH = 7, then use an ultrasonic cell disruptor (S-450D) to ultrasonically break it for 10 min (50W), then ultrasonically disperse for 30 min, and freeze-dry to obtain For microcrystalline cellulose with a particle size of about 1-10 μm, a certain mass of acid-h...

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Abstract

The invention discloses a wax-based blade coating patterning method which comprises the following steps: performing hydrophilic treatment on the surface of a plastic piece to serve as a substrate; designing a photonic crystal pattern or a pattern of a microfluidic channel, and printing the designed patterns on the substrate by using wax; performing blade coating on SiO2 photonic crystal colloid on the substrate printed with the photonic crystal pattern, so that the SiO2 photonic crystal colloid is poured into a hollow area without the wax; or performing blade coating on microcrystalline cellulose suspension subjected to acidolysis on the substrate printed with the microfluidic channel, so that the microcrystalline cellulose suspension subjected to acidolysis is poured into the hollow area without the wax; and volatilizing a solvent, and forming a SiO2 photonic crystal or a microfluidic chip. The used blade coating has the advantages that the operation is simple, and heating is not needed; the manufactured photonic crystal pattern has excellent optical properties with ordered structure and angle deflection and can be applied to manufacturing anti-counterfeiting patterns, and the manufactured microfluidic chip has the characteristics of high resolution ratio, high flow velocity, low sample consumption and the like and can be used for low-cost biochemical field detection.

Description

technical field [0001] The invention belongs to the field of micromachining, and specifically relates to a wax-based scraping patterning method, that is, scraping an aqueous solution suspension on a hydrophilic substrate covered with wax, so as to pattern the material on the hydrophilic surface. Using this method, patterned photonic crystals and cellulose were successfully prepared and applied to the fabrication of fast and high-precision paper microfluidic analysis chips. Background technique [0002] Surface patterning refers to a micromachining method that generates micron or nanoscale regular surface structures in at least one dimension, and is widely used in microreactors, microarray devices, and microfluidic chips. Surface patterning methods include photolithography, micromechanical methods based on scanning probes, microcontact printing, inkjet printing, etc. Wax-based patterning methods mainly include screen printing, wax spray printer direct printing, etc. [0003...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B81C1/00B01L3/00
Inventor 刘宏高兵兵顾忠泽
Owner SOUTHEAST UNIV
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