Zirconium-based alloy ingot and preparation method thereof as well as prepared zirconium-based amorphous alloy
A technology for zirconium-based alloys and alloy ingots, which is applied in the field of alloy ingots, and can solve the problems of unintroduced zirconium-based alloy ingot preparation methods and inability to obtain zirconium-based alloy ingots, etc., and achieve the effect of cooling speed suppression
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Embodiment 1
[0043] A zirconium-based alloy ingot, the zirconium-based alloy ingot is composed of the following atomic percent atoms:
[0044] Zr 65%
[0045] Cu 15%
[0046] Ni 8%
[0047] Al 9%
[0048] Nb 3%.
[0049] A method for preparing a zirconium-based alloy ingot, comprising the following steps:
[0050] Step A, preparation of the master alloy: Melting the Nb metal and part of the Ni metal required for the zirconium-based alloy ingot by vacuum arc melting method to obtain the master alloy. The preparation of the master alloy in the step A specifically includes the following steps:
[0051] Step A1, before melting: pump the melting chamber of the vacuum arc melting furnace to 10 -4 torr vacuum degree, then pour high-purity argon into the melting chamber, and the amount of high-purity argon is 60% of the volume of the melting chamber;
[0052]Step A2, during melting: mix the Nb metal and Ni metal required for the zirconium-based alloy ingot at a weight ratio of 51:49, and m...
Embodiment 2
[0062] A zirconium-based alloy ingot, the zirconium-based alloy ingot is composed of the following atomic percent atoms:
[0063] Zr 50%
[0064] Cu 20%
[0065] Ni 17%
[0066] Al 5%
[0067] Nb 8%.
[0068] A method for preparing a zirconium-based alloy ingot, comprising the following steps:
[0069] Step A, preparation of the master alloy: Melting the Nb metal and part of the Ni metal required for the zirconium-based alloy ingot by vacuum arc melting method to obtain the master alloy. The preparation of the master alloy in the step A specifically includes the following steps:
[0070] Step A1, before melting: pump the melting chamber of the vacuum arc melting furnace to 10 -4 torr vacuum, then pour high-purity argon into the melting chamber, the amount of high-purity argon is 80% of the volume of the melting chamber;
[0071] Step A2, when melting: mix the Nb metal and Ni metal required for the zirconium-based alloy ingot at a weight ratio of 51:49, and melt at a te...
Embodiment 3
[0081] A zirconium-based alloy ingot, the zirconium-based alloy ingot is composed of the following atomic percent atoms:
[0082] Zr 57%
[0083] Cu 15.4%
[0084] Ni 12.6%
[0085] Al 10%
[0086] Nb 5%.
[0087] A method for preparing a zirconium-based alloy ingot, comprising the following steps:
[0088] Step A, preparation of the master alloy: Melting the Nb metal and part of the Ni metal required for the zirconium-based alloy ingot by vacuum arc melting method to obtain the master alloy. The preparation of the master alloy in the step A specifically includes the following steps:
[0089] Step A1, before melting: pump the melting chamber of the vacuum arc melting furnace to 10 -4 torr vacuum degree, then pour high-purity argon into the melting chamber, and the amount of high-purity argon is 70% of the volume of the melting chamber;
[0090] Step A2, when melting: mix the Nb metal and Ni metal required by the zirconium-based alloy ingot at a weight ratio of 51:49, a...
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