Modified asphalt, method for preparing modified asphalt by using direct liquefied coal residue in normal pressure continuous mode and application of modified coal residue
A technology for direct liquefaction of coal and modified asphalt, which is applied in the processing of tar pitch/petroleum pitch/natural pitch, chemically processing tar pitch/petroleum pitch/natural pitch, and processing tar pitch/petroleum pitch/natural pitch by selective extraction In other directions, it can solve the problems of increasing the complexity of the process and the inability to carry out continuous production, and achieve the effect of good market application prospects, strong development applicability, and pollution reduction.
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[0044] 1) Add 300Kg coal direct liquefaction residue and extraction solvent vacuum residue (distillation range: 300-420°C) into the stirred tank (the weight ratio of coal direct liquefaction residue to vacuum residue is 1:2.5), at 60r / min speed stirring to obtain a mixture. Fill the stirred tank with N 2 When the pressure in the stirred tank was raised to 0.1 MPa, the temperature of the mixture was raised to 150°C at 20°C / hour, then stirred at a constant temperature of 300r / min, and subjected to hot-solution extraction for 30min to obtain an extraction mixture.
[0045] 2) Solid-liquid separation of the extraction mixture is carried out by means of hot-press filtration. The filtration temperature is 150° C., the filtration pressure is 0.3 MPa, and the pore size of the filter core is 30 μm. After filtration, the extract and raffinate were collected.
[0046] 3) Send the extract to a vacuum distillation tower for vacuum distillation to recover the solvent. The temperature at...
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