Treatment method of standard exceeding of content of chlorine in titanium sponge
A treatment method and technology of sponge titanium, which is applied in the field of sponge titanium production, can solve problems such as the blockage of the middle channel of the distillation tank, the chlorine element of sponge titanium exceeds the standard, and affect the quality of sponge titanium, so as to reduce the chlorine content and improve the grade rate.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
example 1
[0033] Put the whole lump of titanium sponge into the reactor that has been produced and cleaned, seal the bottom of the reactor with a blind plate, seal the reactor with a tank cover and evacuate the reactor to 60Pa for air tightness leak test, and pass Finally, put the reactor equipped with titanium sponge into a vacuum electric furnace, and degas at a low temperature of 150-200°C for 3 hours under the condition of a vacuum of 60Pa; then degas at a medium temperature, and the temperature is controlled at 250-300°C according to the successive stages , 350 ~ 400 ℃, 450 ~ 500 ℃, 500 ~ 550 ℃ four constant temperature section, and each constant temperature 2h. After the degassing is completed, raise the temperature of the electric furnace to 900-1020°C and continue vacuum distillation. During the distillation process, air convection is used to cool the distillate naturally. When the constant temperature is 37 hours at 900-1020°C, the vacuum degree in the reactor is <4 Pa for 7 hou...
example 2
[0036] Put the sponge titanium crushed to a particle size of 0.83-25.4mm into the reactor that has been produced and cleaned, seal the bottom of the reactor with a blind plate, seal the reactor with a tank cover, and evacuate the reactor to 90Pa for gas Leakage test for tightness. After passing the test, place the reactor with titanium sponge into a vacuum electric furnace, and degas at a low temperature of 150-200°C for 5 hours under a vacuum of 90 Pa; The stage control is 250~300℃, 350~400℃, 450~500℃, 500~550℃ four constant temperature sections, and each constant temperature is 3h. After the degassing is completed, raise the temperature of the electric furnace to 900-1020°C and continue the vacuum distillation at a constant temperature. During the distillation process, use air convection to cool the distillate naturally. When the vacuum degree in the reactor is less than 15Pa for 6 hours, and the distillation time is 53 hours, stop the heating reaction Fill the reactor with ...
PUM
Property | Measurement | Unit |
---|---|---|
particle size | aaaaa | aaaaa |
Brinell hardness | aaaaa | aaaaa |
Brinell hardness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com