Preparation method of environment-friendly PU (polyurethane) ceiling with flame retardant and sound absorption functions
A polyurethane and environmentally friendly technology, applied in the field of polymer chemical materials, to achieve the effects of low overall cost, low board density, and less material consumption
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[0025]The invention provides a method for preparing an environment-friendly polyurethane flame-retardant sound-absorbing ceiling. Polyester-type isocyanate prepolymer is used as an adhesive, mixed evenly with pulverized waste polyurethane rigid foam particles, and then molded into an environment-friendly polyurethane insulation ceiling. Sound-absorbing ceiling, wherein, the polyester-type isocyanate prepolymer is 5-10 parts by weight, the crushed waste polyurethane rigid foam particles is 90-95 parts by weight, and the polyester-type isocyanate prepolymer is An isocyanate prepolymer with an NCO content of 10-30% is prepared by reacting diisocyanate and polyester polyol at 60-80°C.
[0026] Wherein, a better processing flow using the method of the present invention is:
[0027] (1) a. Prepare polyester type isocyanate prepolymer;
[0028] The isocyanate prepolymer with an NCO content of 10-30% is prepared by reacting diisocyanate and polyester polyol at 60-80°C; among them...
Embodiment 1
[0053] Put 5.0kg of PMDI and 3.9kg of PEDA1500 into the reaction kettle, control the temperature at 60~65°C for 3~4h, discharge, and detect that the NCO content is 15.1%, and obtain a qualified polyester isocyanate prepolymer;
[0054] Pulverize the waste polyurethane rigid foam into particles below 10 mesh through a pulverizer;
[0055] Put 12 kg of waste polyurethane rigid foam particles into the mixer, start stirring to make the above particles roll in the equipment, spray evenly into 1 kg of the above-mentioned prepared polyester isocyanate prepolymer, stir and mix evenly;
[0056] Spread the mixture obtained above evenly into a mold of 2.00×1.00×0.02m between the heating plates of the press, and perform a preheating treatment at 100°C for 5 minutes; then, start the pressure to 15MPa, and then hold Press for 15 minutes, demould, and get the environment-friendly polyurethane flame-retardant sound-absorbing ceiling.
[0057]
Embodiment 2
[0059] Put 5.0kg of PMDI and 0.158kg of PEDA2000 into the reaction kettle, control the temperature at 60~65°C for 3~4h, discharge the material, and detect that the NCO content is 30.0%, and obtain a qualified polyester isocyanate prepolymer;
[0060] Pulverize the waste polyurethane rigid foam into particles below 10 mesh through a pulverizer;
[0061] Put 13.68kg of waste polyurethane rigid foam particles into the mixer, start stirring to make the above particles roll in the equipment, spray evenly into 0.72kg of the above-mentioned polyester isocyanate prepolymer, stir and mix evenly;
[0062] Spread the mixture obtained above evenly into a mold of 2.00×1.00×0.02m between the heating plates of the press, and perform a preheating treatment at 120°C for 5 minutes. At the same time, place PVC leather veneer materials on both sides of the mold; then, start The pressure is increased to 20 MPa, and then the pressure is maintained at 120°C for 20 minutes, and the mold is demoulded ...
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