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Paeonol extracting method

A paeonol extraction technology, applied in the field of paeonol extraction, can solve the problems of high energy consumption, long production cycle, and high equipment cost, and achieve the effects of improving economic benefits, high recovery rate, and simple method

Active Publication Date: 2014-02-05
安徽德昌药业股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Alcohol extraction and steam distillation have the defects of high energy consumption, long production cycle and low yield
CO 2 Although the supercritical fluid extraction method has high extraction efficiency, it is difficult to industrialize production due to the high cost of equipment

Method used

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Examples

Experimental program
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Effect test

Embodiment Construction

[0010] Paeonol extraction method, take Moutan cortex or Xu Changqing medicinal materials, crush them, put them into the extraction kettle, pass in carbon dioxide pressurized liquid into the extraction kettle, and soak for 1-1.2 hours at a temperature of 40-60°C; then pour into the extraction kettle Add alcohol to extract, place and crystallize to get paeonol, carbon dioxide pressurized pressure 20 ~ 40Mpa, the ratio of the weight (g) of Moutan cortex to the volume (ml) of alcohol is 1:5.

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PUM

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Abstract

The invention discloses a paeonol extracting method which comprises the following steps: grinding moutan bark or cynanchum paniculatum, putting into an extracting kettle, filling the extracting kettle with carbon dioxide pressurizing liquid, and soaking at the temperature of 40-60 DEG C for 1-1.2 hours; adding alcohol into the extracting kettle for extraction, and standing for crystallizing to obtain paeonol. The method is simple, novel, high in recovery rate during extraction, stable in ingredients and high in economic benefit.

Description

technical field [0001] The invention relates to the technical field of paeonol extraction, in particular to a paeonol extraction method. Background technique [0002] Paeonol is the main active ingredient in Moutan cortex. It is volatile and can be distilled out with water vapor under a certain vapor pressure. It is a colorless needle-like crystal at room temperature, and its solubility in water is very low. The current experimental research shows that the main pharmacological effects of Cortex Moutan are relatively extensive. With the rise of traditional Chinese medicine and the increasing material and cultural level of the people, the demand for health care products has greatly increased, and the country has attached great importance to traditional Chinese medicine, which has greatly promoted the development and recognition of traditional Chinese medicine technology. At present, the domestic demand for paeonol is 160-200 tons, most of which depend on imports. In terms of ...

Claims

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Application Information

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IPC IPC(8): C07C49/84C07C45/80
CPCC07C45/78C07C49/84
Inventor 葛德州孙伟修效友
Owner 安徽德昌药业股份有限公司
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