Hydrogen fuel cell polymer film and preparation method thereof
A polymer membrane and fuel cell technology, applied in fuel cells, fuel cell parts, circuits, etc., can solve the problems of restricting technological upgrading and industrial development, and achieve the effect of high conductivity and good application space
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Embodiment 1
[0007] (1) Take 15g of polyaniline, dissolve it in 30g of ethanol, stir slowly, dissolve evenly, and set aside; (2) Take 3g of triethylenediamine, dissolve it with 20g of acetone, stir evenly for 3h, set aside (3) Take 4 g of styrene oxide, dissolve it with 15 g of ether, and seal it for use after dissolving evenly; (4) Pour the solution obtained in steps (1), (2), and (3) into vacuum and reduce pressure In the distiller, the temperature is 50°C, distill under reduced pressure until all the solvent evaporates, and stop when no more solvent flows out; (5) Soak the polymer film after the solvent evaporates in distilled water for 12 hours; (6) After soaking, the polymer film The membrane is taken out from the water and dried at 80°C, which is the hydrogen fuel cell polymer membrane.
Embodiment 2
[0009] (1) Take 12g of polyaniline, dissolve it in 35g of ethanol, stir slowly, dissolve evenly, and set aside; (2) Take 4g of triethylenediamine, dissolve it with 20g of acetone, stir evenly for 2 hours, and set aside (3) Take 2 g of styrene oxide, dissolve it with 25 g of ether, and seal it up for use after dissolving evenly; (4) Pour the solution obtained in steps (1), (2), and (3) into vacuum pressure In the distiller, the temperature is 50°C, distill under reduced pressure until all the solvent evaporates, and stop when no more solvent flows out; (5) soak the polymer film after the solvent evaporates in distilled water for 10 hours; (6) soak the polymer film after immersion The membrane is taken out from the water and dried at 80°C, which is the hydrogen fuel cell polymer membrane.
Embodiment 3
[0011] (1) Take 13g of polyaniline, dissolve it in 40g of ethanol, stir slowly, dissolve evenly, and set aside; (2) Take 5g of triethylenediamine, dissolve it with 15g of acetone, stir evenly for 1h, and set aside (3) Take 3 g of styrene oxide, dissolve it with 15 g of ether, and seal it up for use after dissolving evenly; (4) Pour the solution obtained in steps (1), (2), and (3) into vacuum pressure reduction In the distiller, the temperature is 50°C, distill under reduced pressure until all the solvent evaporates, and stop when no more solvent flows out; (5) soak the polymer film after the solvent evaporates in distilled water for 8 hours; (6) soak the polymer film after immersion The membrane is taken out from the water and dried at 80°C, which is the hydrogen fuel cell polymer membrane.
[0012] The electronic conductivity of the hydrogen fuel cell polymer membranes prepared according to Example 1, Example 2, and Example 3 was measured. The electronic conductivity of Exam...
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