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Diacetylene-class thermochromic ink and method for preparing same

A thermochromic ink and thermochromic technology, used in inks, household appliances, applications, etc., can solve the problems of ink containing toxic and harmful substances, secondary pollution, etc., and achieve uniform dispersion of color components, saving consumption, and simple equipment. Effect

Active Publication Date: 2014-01-08
THE 724TH RES INST OF CHINA SHIPBUILDING IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Technical problem to be solved: Aiming at the shortcomings of traditional temperature-sensitive color-changing inks that contain toxic and harmful substances and are likely to cause secondary pollution, the present invention provides an irreversible temperature-changing ink Diacetylene temperature-sensitive color-changing ink and preparation method thereof

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A diacetylene thermosensitive color-changing ink is composed of the following raw materials in parts by mass:

[0030] 10 parts of 10,12-pentacosadiynoic acid;

[0031] 45 parts of tung oil;

[0032] Calcium carbonate 25 parts;

[0033] 15 parts of barium sulfate;

[0034] Annatto pigment 5 parts.

[0035] A preparation method of diacetylenic temperature-sensitive color-changing ink, comprising the following steps:

[0036] (1) Mixing: Add diacetylene-based thermochromic materials to tung oil, use an ink knife to manually stir, add annatto pigment while stirring as needed, and stir for 2 minutes to form a mixture;

[0037] (2) Heating: heat the mixture in a microwave oven for 15 seconds to raise the temperature of the mixture to 55°C, continue stirring manually with an ink knife for 1 minute, and heat it in the microwave oven again for 15 seconds to raise the temperature of the mixture to 55°C;

[0038] (3) Add filler: add calcium carbonate and barium sulfate to th...

Embodiment 2

[0041] A diacetylene thermosensitive color-changing ink is composed of the following raw materials in parts by mass:

[0042] 15 parts of 10,12-trisosadiynoic acid;

[0043] 50 parts of linseed oil;

[0044] 22 parts of calcium carbonate;

[0045] Barium sulfate 13 parts.

[0046] A preparation method of diacetylenic temperature-sensitive color-changing ink, comprising the following steps:

[0047] (1) Mixing: add diacetylenic thermochromic material to linseed oil, use ink knife to manually stir, and stir for 2 minutes to form a mixture;

[0048] (2) Heating: Heat the mixture in a microwave oven for 15s to raise the temperature of the mixture to 50°C, use an ink knife to continue stirring by hand for 2 minutes, put it into the microwave oven again and heat for 15s to raise the temperature of the mixture to 50°C;

[0049] (3) Add filler: add calcium carbonate and barium sulfate to the heated mixture at the same time, stir with an ink knife for 2-4 minutes, until the viscosi...

Embodiment 3

[0052] A diacetylene thermosensitive color-changing ink is composed of the following raw materials in parts by mass:

[0053] 5 parts of 10,12-pentacosadiynoic acid;

[0054] 5 parts of 10,12-trisosadiynoic acid;

[0055] 40 parts of tung oil;

[0056] Calcium carbonate 25 parts;

[0057] 10 parts of barium sulfate;

[0058] Capsanthin 5 parts.

[0059] A preparation method of diacetylenic temperature-sensitive color-changing ink, comprising the following steps:

[0060] (1) Mixing: Add diacetylene-based thermochromic materials to tung oil, use an ink knife to manually stir, add capsanthin while stirring as needed, and stir for 2 minutes to form a mixture;

[0061](2) Heating: heat the mixture in a microwave oven for 15 seconds to raise the temperature of the mixture to 60°C, continue to stir manually for 1 minute with an ink knife, and heat it in the microwave oven again for 15 seconds to raise the temperature of the mixture to 60°C;

[0062] (3) Add filler: add calcium...

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Abstract

The invention provides diacetylene-class thermochromic ink and a method for preparing the diacetylene-class thermochromic ink. The diacetylene-class thermochromic ink is formed by the raw materials of, by mass, 8-15 parts of diacetylene-class thermochromic materials, 40-50 parts of vegetable oil type varnish, 20-25 parts of calcium carbonate and 10-15 parts of barium sulfate. The diacetylene-class thermochromic ink is even in color component dispersion, strong in viscosity with print and fadeless, equipment used in the preparing process is simple, the ink can be transformed into mass production and is easy to popularize, productivity is formed, food grade materials are selected and used as raw and auxiliary materials according to rules, and the ink can be used for food package printing.

Description

technical field [0001] The invention belongs to the field of screen printing inks for paper, and in particular relates to a diacetylene temperature-sensitive color-changing ink and a preparation method thereof. Background technique [0002] Thermochromic inks have been widely used in daily life, but most of them contain toxic or harmful substances, which are restricted when used in the field of food or food packaging materials. Usually, reusable packaging containers for food or medicine need to be sterilized at high temperature. During disinfection, real-time monitoring of the disinfection effect is required. Since the containers are stacked together during disinfection, they will affect each other, and some containers cannot reach the temperature set for disinfection, but the disinfection effect cannot be judged intuitively. In addition, if the traditional temperature-sensitive color-changing ink is used, it is easy to cause secondary pollution, and the purpose of disinfec...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D11/06
CPCC09D11/06C09D11/03C09D11/50
Inventor 吴兴旺李进吴立丰贺力王仕杰张鹏
Owner THE 724TH RES INST OF CHINA SHIPBUILDING IND
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