Peony and liquorice soup formula granule, preparation method and detection method of peony and liquorice soup formula granule
A technology of Shaoyao Gancao Decoction and formula granules, which is applied in the directions of pharmaceutical formulations, medical preparations containing active ingredients, antipyretics, etc., can solve the problems of Shaoyao Gancao Decoction formula granules that cannot be used safely and the quality cannot be well controlled.
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Embodiment 1
[0084] Preparation of Example 1 Shaoyao Gancao Decoction Formula Granules
[0085] 1. Source of medicinal materials
[0086] See Table 1 for source and place of origin
[0087] Table 1 sources of medicinal materials
[0088]
[0089] 2. Instruments and equipment
[0090] Midea Induction Cooker; RE-5205 Rotary Evaporator, Shanghai Yarong Biochemical Instrument Factory; KQ-300VDB Dual-Frequency CNC Ultrasonic Cleaner, Kunshan Ultrasonic Instrument Co., Ltd.; B-290 Spray Dryer, Buchi, Switzerland.
[0091] 3. Preparation method
[0092] 2400g of peony, 2400g of roasted licorice, made into 1000g granules.
[0093] Preparation process of formula granules of Shaoyao Gancao Decoction: decoct peony and licorice, filter the decoction; combine the filtrates, concentrate to a concentrated solution with a relative density of about 1.08-1.18 (60°C), spray dry, and make a dry extract powder. Add an appropriate amount of water, granulate, and sieve to obtain the formula granules of...
Embodiment 2
[0106] Embodiment 2 Thin-layer chromatography identification embodiment 1 is A in process condition 2 B 1 C 2 peony Herbal Licorice Decoction Formula Granules
[0107] 1. Identification of Radix Paeoniae Alba in Formula Granules of Shaoyao Gancao Decoction
[0108] 1.1 Reagents and Reagents
[0109] Radix Paeoniae Alba reference medicinal material: batch number 120905-200407, purchased from China Institute for the Control of Pharmaceutical and Biological Products;
[0110] Paeoniflorin reference substance: batch number 10736-200735, purchased from China Institute for the Control of Pharmaceutical and Biological Products;
[0111] Test product: batch numbers 20110914, 20120101, 20120102, 20120103, produced by Kangmei Pharmaceutical Research Institute according to the process conditions described in Example 1. 2 B 1 C 2 when the method is prepared;
[0112] Thin-layer board: Silicone G thin-layer board (Qingdao).
[0113] Reagents are analytically pure ...
Embodiment 3
[0160] Embodiment 3 detects that embodiment 1 is A at process condition 2 B 1 C 2 Shaoyao Gancao Decoction prepared in time Heavy metal content of square particles
[0161] For the detection items, refer to the Chinese Pharmacopoeia 2010 edition, one Huanglian Shangqing Pill [check] item, take about 1 g of the Shaoyao Gancao Decoction formula granules prepared in Example 1, accurately weigh it, and check the residue on ignition according to the Chinese Pharmacopoeia 2010 edition one Appendix IXJ) Burn until completely ashed. Take the remaining residue and check according to the second method (Appendix IX E of the Chinese Pharmacopoeia 2010 Edition), the results show that the weight percentage of heavy metals does not exceed 25ppm.
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