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Production method of metal lead powder applied in nuclear engineering field

A production method and metal lead technology are applied in the production of metal powder and the atomization production of metal lead powder, which can solve the problems of lead powder and tin powder being easy to agglomerate, easy to oxidize and deteriorate, and heavy metal poisoning, etc., so as to improve the working environment. , Significant economic benefits, the effect of reducing production costs

Inactive Publication Date: 2013-06-05
重庆华浩冶炼有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Since the metal lead powder produced by the atomization method is easily oxidized and deteriorated when exposed to the air, vacuum packaging is used, but the products produced under the existing production technology conditions have the following problems: 1. Vacuum packaging is prone to various leaks 2. Due to the difference in internal and external pressure in vacuum packaging, lead powder and tin powder are easy to agglomerate; 3. The reprocessing of oxidized and agglomerated powder increases a lot of cost, and at the same time, the volatilization and flying of powder causes Metal loss, volatilization and flying can also easily cause heavy metal poisoning

Method used

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  • Production method of metal lead powder applied in nuclear engineering field
  • Production method of metal lead powder applied in nuclear engineering field

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Effect test

Embodiment 1

[0017] A kind of production method of metallic lead powder, carry out according to the following steps:

[0018] a. Dissolving in a metal melting furnace to obtain a metal lead liquid flow, the temperature of the molten lead liquid is controlled at 475-485°C;

[0019] b. The diameter of the metal lead liquid added in the atomization process is 2-2.5mm; the pressure is 0.7-0.9Mpa, and the air flow is 9-10.5m 3 The high-pressure air of / min is fed into the atomizing equipment to atomize the metal lead liquid flow, and simultaneously feeds the benzotriazole additive, and the added amount of the benzotriazole additive accounts for 10% of the metal liquid flow weight entering the atomizing equipment 0.04% to 0.055%, the addition temperature of the benzotriazole additive is 264 to 275°C, and the pressure is 0.8 to 0.95 standard atmospheres;

[0020] c. Cool to normal temperature and collect powder;

[0021] d. Sieved, packaged into bags for standby or for sale.

[0022] The above...

Embodiment 2~6

[0023] Embodiment 2~6: Produce metal powder according to following steps and process, all the other are the same as embodiment 1.

[0024]

[0025] The oxidative deterioration rate of the 0.050mm grade metal lead powder prepared by the above method is only 1.2-3%, and it is packaged conventionally, and the economic benefit is remarkable; the safety in the preparation process is good.

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Abstract

Provided is a production method of metal lead powder applied in the nuclear engineering field. The production method includes steps of metal melting and metal atomization. The temperature of melting lead liquid is controlled at about 470-490 celsius degrees in the process of metal melting. Thiazole additive is added in the process of metal atomization, and the addition amount of the thiazole additive is 0.02%-0.07% of the melted metal lead liquid. High-pressure air flows into the metal atomization process is controlled at 9-10.5 cubic meters per minute. According to the production method of metal lead powder applied in the nuclear engineering field, a kind of additive is chosen in the process of metal lead powder production through atomization, and self property of the additive, interaction between the additive and metals, and the advantageous environment of atomization are utilized, so that the additive is gasified to form a protective layer on the metal lead powder surface to prevent oxidation and agglomerate. Lead powder products produced by using the method and with conventional packing, oxidation rate of the metal lead powder products can be effectively controlled at 0.5% -4%. With the conventional packing, production cost is effectively lowered and security of production system is good. Return rate is greatly reduced, and economic benefit is remarkable.

Description

technical field [0001] The invention relates to a production method of metal powder, in particular to an atomization production method of metal lead powder, belonging to the technical field of metallurgy. Background technique [0002] At present, the production of metal lead powder adopts the gas atomization method, and its basic production process is: the first step, the melting of the metal, the melting temperature is 50 ° C to 100 ° C higher than the melting point of the metal; the second step, in the atomization equipment, use 0.3MP~1.2MP high-pressure air atomizes the metal liquid flow to produce powder that meets the corresponding specifications and requirements; the third step is to cool and collect the powder; the fourth step is to sieve the cooled powder; the fifth step is to vacuum the product Package. [0003] Since the metal lead powder produced by the atomization method is easily oxidized and deteriorated when exposed to the air, vacuum packaging is used, but t...

Claims

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Application Information

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IPC IPC(8): B22F9/08B22F1/00
Inventor 曾明军王绪其莫正彬
Owner 重庆华浩冶炼有限公司
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