Application of ulva polysaccharide in cigar
A kind of Ulva polysaccharide, cigarette technology, applied in the field of cigarette additives
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Embodiment 1
[0020] The raw materials were cleaned and removed, dried and pulverized to obtain Ulva dry powder, added 10 times the weight of water, soaked at room temperature for 2 hours, heated to 45°C, added 0.5% cellulase and 0.2% protease by weight of Ulva dry powder, 45 Keep at ℃ for 2 hours, heat up to 70 ℃ and reflux for 5 hours, stop heating and filter, the clear liquid is concentrated under reduced pressure to obtain a concentrated solution, add 3 times the volume of 95% ethanol until the ethanol concentration of the system is 60%, let it stand for 24 hours, and the precipitate is freeze-dried Ulva polysaccharides were obtained.
[0021] The Ulva polysaccharide is dissolved in water, sprayed evenly on the shredded tobacco according to 0.01% of the weight of the shredded tobacco, baked and rolled into cigarettes. The results of the smoking test show that the smoke has no peculiar smell, the miscellaneous gas is reduced, and the aftertaste is improved.
Embodiment 2
[0023] The raw materials were washed, removed, dried and pulverized to obtain Ulva dry powder, added 12 times the weight of water, soaked at room temperature for 3 hours, heated to 50°C, added 1% cellulase and 0.3% protease by weight of Ulva dry powder, 50 Keep at ℃ for 1.5h, heat up to 80℃ and reflux for 4h, stop heating and filter, the clear liquid is concentrated under reduced pressure to obtain a concentrated solution, add 4 times the volume of 95% ethanol until the ethanol concentration of the system is 70%, let it stand for 24h, and freeze the precipitate Dried Ulva polysaccharide.
[0024] The Ulva polysaccharide is dissolved in water, sprayed evenly on the shredded tobacco according to 0.001% of the weight of the shredded tobacco, baked and rolled into cigarettes. The results of the smoking test show that the smoke has no peculiar smell, the miscellaneous gas and irritation are reduced, the aftertaste is clean, and it has a sense of body fluid.
Embodiment 3
[0026] The raw materials were cleaned, removed, dried and pulverized to obtain Ulva dry powder, adding 15 times the weight of water, soaking at room temperature for 4 hours, heating to 55°C, adding 2% cellulase and 0.5% protease by weight of Ulva dry powder, 55 Keep at ℃ for 1h, heat up to 90℃ and reflux for 3h, stop heating and filter, the clear liquid is concentrated under reduced pressure to obtain a concentrated solution, add 5 times the volume of 95% ethanol until the ethanol concentration of the system is 80%, let it stand for 24h, and the precipitate is freeze-dried Ulva polysaccharides were obtained.
[0027] The Ulva polysaccharide is dissolved in water, sprayed evenly on the shredded tobacco according to 0.005% of the weight of the shredded tobacco, baked and rolled into cigarettes. The results of the smoking test show that the smoke has no peculiar smell, the miscellaneous gas and irritation are reduced, and it has a sense of body fluid.
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