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Ultrahigh pressure extraction method of asparagus saponin

An extraction method and ultra-high pressure technology, which are used in pharmaceutical formulations, solid solvent extraction, medical preparations containing active ingredients, etc., can solve the problems of low active ingredient activity, low extraction efficiency, and high extraction temperature, and achieve high active ingredient activity. , The effect of high extraction efficiency and low extraction temperature

Inactive Publication Date: 2014-09-10
四川秦巴山珍食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The present invention aims to solve the problems of long extraction time, low extraction efficiency, large energy consumption, high extraction temperature and low activity of extracted active ingredients in the existing extraction method of asparagus saponin, and provides an ultra-high pressure extraction of asparagus saponin method, this method can solve the above problems, achieve the purpose of improving efficiency and improving the activity of active ingredients, and can make the extraction rate of asparagus saponin reach more than 0.77%, and the product purity reach more than 85%

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] An ultra-high pressure extraction method of asparagus saponin, comprising the following process steps:

[0037] A. Raw material handling

[0038] Remove asparagus from debris, wash and set aside;

[0039] B. Dry and crush

[0040] Drying the processed asparagus and crushing it into asparagus powder;

[0041] C. Degreasing

[0042] Add chloroform to the asparagus powder obtained in step B, reflux extraction, then filter to remove the filtrate, and obtain the degreased asparagus product after the filter residue is evaporated to dryness, and set aside;

[0043] D. Ultra-high pressure extraction

[0044] Select n-butanol aqueous solution as the extraction solvent to carry out ultra-high pressure extraction at normal temperature, the mass ratio of the extraction solvent to the degreased asparagus product is 65:1, the extraction pressure is 200MPa, and the solvent in the extract is recovered after holding the pressure for 2 minutes to obtain the ultra-high pressure Extra...

Embodiment 2

[0050] An ultra-high pressure extraction method of asparagus saponin, comprising the following process steps:

[0051] A. Raw material handling

[0052] Remove asparagus from debris, wash and set aside;

[0053] B. Dry and crush

[0054] Drying the processed asparagus and crushing it into asparagus powder;

[0055] C. Degreasing

[0056] Add chloroform to the asparagus powder obtained in step B, reflux extraction, then filter to remove the filtrate, and obtain the degreased asparagus product after the filter residue is evaporated to dryness, and set aside;

[0057] D. Ultra-high pressure extraction

[0058] Select n-butanol aqueous solution as the extraction solvent to carry out ultra-high pressure extraction at normal temperature, the mass ratio of the extraction solvent to the degreased asparagus product is 70:1, the extraction pressure is 300MPa, and the solvent in the extract is recovered after holding the pressure for 4 minutes to obtain the ultra-high pressure Extra...

Embodiment 3

[0064] An ultra-high pressure extraction method of asparagus saponin, comprising the following process steps:

[0065] A. Raw material handling

[0066] Remove asparagus from debris, wash and set aside;

[0067] B. Dry and crush

[0068] Drying the processed asparagus and crushing it into asparagus powder;

[0069] C. Degreasing

[0070] Add chloroform to the asparagus powder obtained in step B, reflux extraction, then filter to remove the filtrate, and obtain the degreased asparagus product after the filter residue is evaporated to dryness, and set aside;

[0071] D. Ultra-high pressure extraction

[0072] Select n-butanol aqueous solution as the extraction solvent to carry out ultra-high pressure extraction at normal temperature, the mass ratio of the extraction solvent to the degreased asparagus product is 67.5:1, the extraction pressure is 250MPa, and the solvent in the extract is recovered after holding the pressure for 3 minutes to obtain the ultra-high pressure Ext...

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Abstract

The invention relates to an ultra-high pressure extraction method of asparagus saponin, which belongs to the technical field of natural products. The process of the present invention includes the steps of raw material treatment, drying and crushing, degreasing, ultra-high pressure extraction, separation and purification, and vacuum evaporation. Mainly by optimizing and improving the ultra-high pressure extraction step, the ultra-high pressure extraction technology combined with the macroporous resin adsorption technology is applied to asparagus The production of saponins effectively solves the technical difficulties in the production of asparagus saponins, so that the produced saponins have the characteristics of high safety, not easy to absorb moisture, good wettability, strong spreadability, excellent adhesion, etc., and the extraction time is short, High extraction efficiency, low energy consumption, low extraction temperature, high activity of active ingredients, environmental protection and no pollution, can effectively extract asparagus saponins in asparagus plants and scraps, and can also extract amino acids in asparagus plants and scraps.

Description

technical field [0001] The invention relates to an extraction method of active ingredients in plants, more specifically, the invention relates to an ultra-high pressure extraction method of asparagus saponin, which belongs to the technical field of natural products. Background technique [0002] Asparagus, also known as Shi Diaobo, is a perennial herb with rich nutrients and has the effect of both medicine and food. For the utilization of asparagus saponin in asparagus, the traditional method is to take its rhizomes and eat them, but a large amount of asparagus plants and leftovers are discarded, causing great waste and affecting the urban and rural environments. However, scientific research has shown that asparagus plants and leftovers have the same active ingredient content as their roots, so extracting asparagus saponins from asparagus roots, plants and leftovers to make high-purity products can make full use of all the effective ingredients in asparagus. Element. [00...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D11/02A61K36/899A61P31/04A61P35/00A23L1/29A61K125/00A23L33/00
Inventor 杨晶
Owner 四川秦巴山珍食品有限公司
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