Preparation method of white fluorescent powder containing europium terbium beryllium polymer

A technology of polymers and phosphors, applied to compounds containing elements of Group 3/13 of the periodic table, chemical instruments and methods, compounds of elements of Group 2/12 of the periodic table, etc., can solve poor color rendering and material selection Insufficient, backward preparation methods and other problems

Active Publication Date: 2013-01-23
SHANXI FEIHONG MICRO NANO PHOTOELECTRONICS SCI & TECH
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AI Technical Summary

Problems solved by technology

[0003] At present, there are three main ways to realize white light LED: one is to use red, green and blue three primary color chips to combine to emit white light. This method requires four electrodes, three driving voltages, and the structure is more complicated; the other is to use blue light chips to excite yellow light fluorescence. Powder, to obtain white light, this phosphor lacks red light components, low color temperature, and poor color rendering; third, use ultraviolet chips to excite three primary color phosphors to obtain white light, this method is easier to obtain white light with the same color, and the light color can be determined by fluorescence The ratio of the powder is determined, and it has the advantages of high color rendering, light color and color temperature adjustment; although these methods can obtain white light, there are also disadvantages of insufficient material selection and backward preparation methods, resulting in white light LEDs that cannot meet the requirements for use.

Method used

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  • Preparation method of white fluorescent powder containing europium terbium beryllium polymer
  • Preparation method of white fluorescent powder containing europium terbium beryllium polymer
  • Preparation method of white fluorescent powder containing europium terbium beryllium polymer

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Embodiment Construction

[0122] The present invention will be further described below in conjunction with accompanying drawing:

[0123] figure 1 As shown in the figure, in order to prepare the state diagram of the white phosphor powder containing europium-terbium-beryllium polymer, the positions of each part must be correct, the ratio should be proportioned, and the operations should be performed in sequence.

[0124] Quantities of chemicals used in preparation are determined in pre-set ranges in grams, milliliters, centimeters 3 is the unit of measurement.

[0125] Preparation of europium-terbium-beryllium polymer white light phosphor is carried out in a four-necked flask under heating, stirring, water bath, water circulation condensation, and nitrogen protection;

[0126] Electric controller 1 top is water bathtub 7, and in water bathtub 7 is water bath water 8, is four-necked flask 9 on water bathtub 7 top, and water bath water 8 will submerge 4 / 5 of four-necked flask volume; From left to rig...

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Abstract

The invention relates to a preparation method of white fluorescent powder containing europium terbium beryllium polymer. The method comprises the steps of: firstly, preparing red europium complex, green beryllium complex and blue beryllium complex; and carrying out polymerization reaction in a four-hole boiling flask, and washing, leaching, drying and grinding to prepare the white fluorescent powder containing the europium terbium beryllium polymer. According to the preparation method, the process is advanced, the data is accurate, the light emitting purity of the white fluorescent powder is good, and the luminous efficiency is high; chromaticity coordinates under 365nm of ultraviolet light excitation are that x is 0.3218 and y is 0.3332, and the preparation method is an ideal method for preparing the white fluorescent powder containing the europium terbium beryllium polymer.

Description

technical field [0001] The invention relates to a preparation method of white light fluorescent powder containing europium-terbium-beryllium polymer, which belongs to the technical field of preparation and application of light-emitting materials. Background technique [0002] Due to its small size, energy saving, environmental protection, long service life, and high luminous efficiency, white LEDs have been widely used in the fields of electronics and lighting, so they are called fourth-generation lighting sources. [0003] At present, there are three main ways to realize white light LED: one is to use red, green and blue three primary color chips to combine to emit white light. This method requires four electrodes, three driving voltages, and the structure is more complicated; the other is to use blue light chips to excite yellow light fluorescence. Powder, to obtain white light, this phosphor lacks red light components, low color temperature, and poor color rendering; thir...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/14C08F230/04C07F5/00C07F3/00C09K11/06
CPCY02B20/181Y02B20/00
Inventor 张爱琴张九丽郝晓东贾虎生刘旭光许并社
Owner SHANXI FEIHONG MICRO NANO PHOTOELECTRONICS SCI & TECH
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