High-efficient cyhalothrin microcapsule suspending agent and preparation method thereof
A technology of high-efficiency cyhalothrin and microcapsule suspension agent, which is applied in the fields of botanical equipment and methods, insecticides, acaricides, etc., can solve problems such as short duration, achieve long duration and save man-hours , exposure toxicity and odor reduction effects
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Embodiment 1
[0027] Example 1: 2% lambda-cyhalothrin microcapsule suspension.
[0028] Preparation method of urea-formaldehyde resin prepolymer aqueous solution: dissolve urea into formaldehyde, the weight ratio of urea and formaldehyde is 1:2.5, adjust the pH value to 8 with sodium hydroxide, stir at a low speed at a temperature of 60°C, and keep warm for 0.5 hours, a viscous and transparent urea-formaldehyde resin is generated, and deionized water equal to the total weight of urea and formaldehyde is added, and stirred at a low speed to obtain a transparent urea-formaldehyde resin prepolymer aqueous solution.
[0029] Dissolve 2% lambda-cyhalothrin completely in 5% xylene at room temperature, add 10% urea-formaldehyde resin prepolymer aqueous solution while stirring, and shear at 2000 rpm for 10 minutes to obtain a stable O / W lotion. Reduce the rotation speed to 1000 rpm, add dilute hydrochloric acid in 5 batches within 1 hour to adjust the pH value to 2.0, polycondensation reaction o...
Embodiment 2
[0030] Example 2: 5% lambda-cyhalothrin microcapsule suspension.
[0031] Preparation method of urea-formaldehyde resin prepolymer aqueous solution: dissolve urea into formaldehyde, the weight ratio of urea and formaldehyde is 1:2, adjust the pH value to 9 with sodium hydroxide, stir at a low speed at a temperature of 80°C, and keep warm for 4 hours, a viscous and transparent urea-formaldehyde resin is generated, and deionized water equal to the total weight of urea and formaldehyde is added, and stirred at a low speed to obtain a transparent urea-formaldehyde resin prepolymer aqueous solution.
[0032] Dissolve 5% lambda-cyhalothrin completely in 12% xylene at room temperature, add 25% urea-formaldehyde resin prepolymer aqueous solution while stirring, and shear at 1500 rpm for 20 minutes to obtain a stable O / W lotion. Reduce the rotation speed to 800 rpm, add dilute hydrochloric acid in 5 batches within 1 hour to adjust the pH value to 2.0, polycondensation reaction occu...
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