Magnetic response photonic crystal anti-fake label and manufacturing method thereof
A photonic crystal and anti-counterfeiting label technology, which is applied to instruments, static indicators, etc., can solve problems such as unfavorable application and low anti-counterfeiting effect, and achieve the effect of low cost, easy operation, and large-scale promotion and use.
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[0048] The invention provides a method for preparing a magnetic response photonic crystal anti-counterfeiting mark, which includes the following steps:
[0049] Mixing the polymerized monomer, the curing agent and the ethylene glycol solution containing carbon-coated superparamagnetic ferroferric oxide colloidal nanoparticles of different particle sizes to obtain a jelly;
[0050] The gel is placed in a plurality of patterns of the anti-counterfeiting mark pattern template, and the magnetic response photonic crystal anti-counterfeiting mark is obtained after the polymerization reaction. A single pattern in the pattern includes at least two kinds of carbon-coated super smooth with different particle sizes Magnetic ferroferric oxide colloidal nanoparticles.
[0051] In the present invention, firstly, ethylene glycol solution containing carbon-coated superparamagnetic ferroferric oxide colloidal nanoparticles of different particle diameters, polymerized monomer and curing agent are stir...
Embodiment 1
[0062] 0.2g of ferrocene was dissolved in 30mL of acetone, and after ultrasonic dispersion, 1.0mL of a 30% mass concentration of hydrogen peroxide aqueous solution was added dropwise to it, and after magnetic stirring was performed at a rotation speed of 1000r / min for 30min, a mixed solution was obtained; The mixed solution was transferred to a 40mL autoclave, sealed and heated to 210°C, and after holding for 72 hours, the reaction system was cooled to room temperature to obtain a black powder; the black powder was washed three times with acetone and ethanol, and then heated at 40°C. Dry in a vacuum oven for 6 hours to obtain a product.
[0063] In the present invention, the obtained product is subjected to transmission electron microscope scanning analysis, and the results are as follows figure 1 As shown, figure 1 This is the TEM image of the carbon-coated superparamagnetic ferroferric oxide colloidal nanoparticles obtained in Example 1 of the present invention. figure 1 It can ...
Embodiment 2
[0070] The ethylene glycol solution of carbon-coated superparamagnetic ferroferric oxide colloidal nanoparticles with a particle size of 125 nm and a particle size of 140 nm in Example 1 was mixed in equal volumes to obtain a mixed solution. Under the action of a magnetic field, the obtained mixed solution immediately appears diffraction phenomenon, and presents a bright color different from that before mixing.
[0071] Mix 0.5 mL of the obtained mixed solution with 2.0 g of polydimethylsiloxane monomer and 0.4 g of curing agent, and stir vigorously for 5 minutes until a uniform gel is formed. Then pour the obtained jelly into a pre-prepared template, and place the template in an oven at 60° C. for polymerization for 2 hours. After curing, a magnetic response photonic crystal anti-counterfeiting mark is obtained.
[0072] The present invention detects the reflection spectrum of the mixed solution, and the result is as follows Figure 7 As shown, Figure 7 Is the reflectance spect...
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