Pyridaben microcapsule suspending agent and preparation method thereof
The technology of a microcapsule suspension and pyridaben, which is applied in the field of pesticides, can solve the problems that the pyridaben microcapsule suspension has not been effectively used, has not fully exerted its efficacy, and is harmful to human health, so as to prolong the effective period of the drug, Consolidate the effect of prevention and control, and the effect of less investment in equipment
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Embodiment 1
[0023] Example 1: 5% pyridaben microcapsule suspension.
[0024] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2, adjust the pH value to 8.5 with 10% sodium hydroxide aqueous solution, stir at a low speed at 70°C, and keep warm for 1 hour to obtain clear and transparent urea - Aqueous solution of formaldehyde resin prepolymer.
[0025] Dissolve 5% pyridaben in 15% xylene, add 2% Nongru 1601# to fully emulsify, stir at 30°C at a speed of 1000 rpm to fully disperse it, and obtain pyridaben mixture solution.
[0026] Add the urea-formaldehyde resin prepolymer aqueous solution to the pyridaben mixture solution stirred at 1000 rpm, stir for 15 minutes to form a stable emulsion, then reduce the stirring rate to 500 rpm, and slowly add an appropriate amount of Acetic acid, adjust its pH value to 5, and the temperature rises to 60°C to solidify the capsule wall. After 2 hours of reaction, the capsule wall is solidified. Use 10% sodium hydroxide aqueo...
Embodiment 2
[0027] Example 2: 10% pyridaben microcapsule suspension.
[0028] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2.5, adjust the pH value to 8.5 with 10% sodium hydroxide aqueous solution, stir at a low speed at 70°C, and keep warm for 1 hour to obtain clear and transparent urea - Aqueous solution of formaldehyde resin prepolymer.
[0029] Dissolve 10% pyridaben in 18% xylene, add 7% Nongru 700# to fully emulsify, stir at 30°C at a speed of 1000 rpm to fully disperse it, and obtain pyridaben mixture solution.
[0030] Add the urea-formaldehyde resin prepolymer aqueous solution to the pyridaben mixture solution stirred at 1000 rpm, stir for 15 minutes to form a stable emulsion, then reduce the stirring rate to 500 rpm, and slowly add an appropriate amount of Acetic acid, adjust its pH value to 5, and the temperature rises to 60°C to solidify the capsule wall. After 2 hours of reaction, the capsule wall is solidified. Use 10% sodium hydroxide a...
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