High-temperature self-propagating curing method for strontium-containing radioactive graphite
A technology of high-temperature self-propagation and solidification method, which is applied in the field of radioactive graphite to achieve the effects of good repeatability, simple technical operation and high production efficiency
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example 1
[0013] Example 1. Graphite, titanium and strontium-containing radioactive graphite (the molar percentage of strontium is 20%) are used as raw materials. Adjust the formula so that the molar ratio of the total amount of graphite to titanium is 0.8:1.2, and the molar ratio of titanium to strontium is 1:0.25. According to the ratio of raw materials to grinding balls of 1:2, zirconium dioxide (ZrO 2 ) balls, and dry milled in a ball mill for 10 hrs in a ball mill. Then, under a pressure of 10 MPa, the mixed and finely processed raw materials were pre-pressed into discs with a diameter of 13 mm. The molded sample was ignited by tungsten wire at ~2200 °C, and the sample was cooled to room temperature after self-combustion to obtain a solidified body of strontium-containing radioactive graphite.
example 2
[0014] Example 2. Graphite, titanium and strontium-containing radioactive graphite (the molar percentage of strontium is 10%) are used as raw materials. Adjust the formula so that the molar ratio of graphite to titanium is 0.8:1.2, and the molar ratio of titanium to strontium is 1:0.1. According to the ratio of raw materials to grinding balls of 1:2.5, zirconium dioxide (ZrO 2 ) balls, and dry milled in a ball mill for 5 hrs in a ball mill. Then, under a pressure of 12 MPa, the mixed and finely processed raw materials were pre-pressed into discs with a diameter of 13 mm. A tungsten wire is used to ignite the molded sample at ~2500 °C, and the sample is cooled to room temperature after self-combustion to obtain a solidified body of strontium-containing radioactive graphite.
example 3
[0015] Example 3. Graphite, titanium and strontium-containing radioactive graphite (the molar percentage of strontium is 30%) are used as raw materials. Adjust the formula so that the molar ratio of graphite to titanium is 1:1, and the molar ratio of titanium to strontium is 1:0.25. According to the ratio of raw materials to grinding balls of 1:2, zirconium dioxide (ZrO 2 ) balls and dry-milled in a ball mill for 7 hrs in a ball mill. Then, under a pressure of 10 MPa, the mixed and finely processed raw materials were pre-pressed into discs with a diameter of 13 mm. The molded sample was ignited by chemical ignition (ignition temperature ~ 2800 ℃), and the sample was ignited by itself and cooled to room temperature to obtain a solidified body of strontium-containing radioactive graphite.
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