Novel high-efficiency composite viscosity reducer for super heavy oil
A technology of oil-soluble viscosity reducer and viscosity reducer, which is applied in the direction of drilling compositions, pipeline systems, chemical instruments and methods, etc., can solve the problem of high cost of using oil-soluble viscosity reducer alone, failure to reduce crude oil viscosity, and In order to improve mining and conveying performance, save mining cost, and control the degree of emulsification
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Embodiment 1
[0029] Embodiment 1. Composite viscosity reducer
[0030] (1) Preparation of oil-soluble viscosity reducer:
[0031] Mixed aromatics (50% by mass): toluene, ethylbenzene (1:1)
[0032] Alcohols (50% by mass): ethanol, octanol, pentanol (1:1:1);
[0033] Preparation method: Mix the above components at normal temperature and pressure, and stir to obtain.
[0034] (2) Preparation of water-soluble viscosity reducer
[0035] Fatty alcohol ether carboxylate is: CH 3 (CH 2 ) 8 O(CH 2 CH 2 O) 8 CH 2 COONa.
[0036] Preparation:
[0037] Add 0.1mol structural formula to the reactor AEOs 8 , under strong stirring and slight heat to dissolve, slowly add 0.253 / 3mol of NaOH powder, this step should pay attention to the feeding speed, to avoid local overheating and darken the color, then add 0.253 / 3mol of NaOH powder after 30 minutes, until NaOH is completely dissolved in alcohol After immersing in ether, start to add 80% chloroacetic acid solution dropwise, and then add the ...
Embodiment 2
[0039] Embodiment 2. Composite viscosity reducer
[0040] (1) Preparation of oil-soluble viscosity reducer:
[0041] Mixed aromatics (50% by mass): toluene, ethylbenzene (1:1)
[0042] Alcohols (50% by mass): ethanol, octanol, pentanol (1:1:1);
[0043] Preparation method: Mix the above components at normal temperature and pressure, and stir to obtain.
[0044] (2) Preparation of water-soluble viscosity reducer
[0045] Fatty alcohol ether carboxylate is: CH 3 (CH 2 ) 8 O(CH 2 CH 2 O) 9 CH 2 COONa.
[0046] Preparation:
[0047] Add 0.1mol structural formula to the reactor AEOs 9 , under strong stirring and slight heat to dissolve, slowly add 0.253 / 3mol of NaOH powder, this step should pay attention to the feeding speed, to avoid local overheating and darken the color, then add 0.253 / 3mol of NaOH powder after 30 minutes, until NaOH is completely dissolved in alcohol After immersing in ether, start to add 80% chloroacetic acid solution dropwise, and then add the ...
Embodiment 3
[0049] Embodiment 3. Composite viscosity reducer
[0050] (1) Preparation of oil-soluble viscosity reducer:
[0051] Mixed aromatics (30% by mass): toluene, ethylbenzene (1:1)
[0052] Alcohols (70% by mass): ethanol, octanol, pentanol (1:1:1);
[0053] Preparation method: Mix the above components at normal temperature and pressure, and stir to obtain.
[0054] (2) Preparation of water-soluble viscosity reducer
[0055] Fatty alcohol ether carboxylate is: CH 3 (CH 2 ) 10 O(CH 2 CH 2 O) 16 CH 2 COONa.
[0056] Preparation:
[0057] The structural formula of adding 0.3mol into the reactor is AEOs 16 , under strong stirring and slight heat to dissolve, slowly add 0.253mol of NaOH powder, this step should pay attention to the feeding speed, in order to avoid local overheating resulting in darkening of the color, then add 0.253mol of NaOH powder after 30 minutes, until NaOH is completely dissolved in alcohol ether Finally, start to add 80% chloroacetic acid solution ...
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