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Preparation method of potassium magnesium salt mine drilling fluid

A drilling fluid and potassium-magnesium salt technology, which is applied in the field of salt mine exploration, can solve the problems of high economic cost, low drilling fluid density, and failure to mine cores, etc., and achieve the effect of improving the recovery rate, simple process, and obvious effect

Inactive Publication Date: 2012-06-27
QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional salt mine drilling fluid is a saturated brine solution, which can prevent fresh water from dissolving the salt mine wall and core, but when drilling into the carnallite (potassium, magnesium chloride) layer, regardless of the Neither saturated brine solution nor saturated potassium salt solution can effectively prevent the drilling fluid from dissolving the wall and core of the carnallite mine, and often the core cannot be mined, or the core is dissolved, which fails to meet the coring requirements
[0003] In the process of carnallite exploration in Laos, diesel oil is also used as drilling fluid, which has a very good effect on the protection of the mine wall and salt core. However, due to the low density of the drilling fluid, the sand in the hole (cuttings, Rock dust) cannot be eliminated in time, and buried drilling accidents are prone to occur when the thickness of the ore layer is large, and on the other hand, the economic cost is high; so this method does not fundamentally solve the drilling fluid problem of carnallite ore
[0004] According to the analysis of the phase diagram of the NaCl-KCl-MgCl2-H2O quaternary system, the composition of the solution at point E of the halite precipitation point at 25°C is 3.35% for KCl, 1.80% for NaCl, and 25.85% for MgCl2. It is not difficult to find that the traditional drilling fluid The reason why carnallite is dissolved is that magnesium chloride is unsaturated, and there is not enough magnesium chloride added to the traditional drilling fluid, so carnallite is dissolved; in addition, traditional salt mine drilling fluid-saturated brine solution has no viscosity, often cuttings and Rock powder cannot be brought out of the drill hole in time, and buried drilling accidents often occur

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Embodiment 1 A kind of preparation method of potassium-magnesium salt ore drilling fluid comprises the following steps:

[0021] (1) Take raw materials by weight ratio (kg / kg): 70% of water, 20% of magnesium chloride, 3% of potassium chloride, 2% of sodium chloride, 4% of bentonite and 1% of carboxymethyl cellulose.

[0022] Wherein: magnesium chloride adopts bischofite (1000kg bischofite contains 540kg of water, magnesium chloride 450kg, potassium chloride 5kg, sodium chloride 5kg); potassium chloride refers to potassium fertilizer with potassium chloride content of more than 95%; sodium chloride is refers to rock salt; bentonite refers to bentonite for drilling mud; carboxymethyl cellulose refers to sodium carboxymethyl cellulose.

[0023] (2) Add water into the stirring tank, then add magnesium chloride, and stir to completely dissolve the magnesium chloride.

[0024] (3) Add potassium chloride and sodium chloride in sequence in the stirring tank, and stir to dissol...

Embodiment 2

[0026] Embodiment 2 A kind of preparation method of potassium-magnesium salt ore drilling fluid comprises the following steps:

[0027] (1) The raw materials are taken by weighing as follows: 68% of water, 20% of magnesium chloride, 1.55% of potassium chloride, 1.11% of sodium chloride, 9% of bentonite and 0.34% of carboxymethyl cellulose.

[0028] Wherein: magnesium chloride adopts bischofite (1000kg bischofite contains 540kg of water, magnesium chloride 450kg, potassium chloride 5kg, sodium chloride 5kg); potassium chloride refers to potassium fertilizer with potassium chloride content of more than 95%; sodium chloride is refers to rock salt; bentonite refers to bentonite for drilling mud; carboxymethyl cellulose refers to sodium carboxymethyl cellulose.

[0029] (2) Add water into the stirring tank, then add magnesium chloride, and stir to completely dissolve the magnesium chloride.

[0030] (3) Add potassium chloride and sodium chloride in sequence in the stirring tank, a...

Embodiment 3

[0032] Embodiment 3 A kind of preparation method of potassium-magnesium salt ore drilling fluid comprises the following steps:

[0033] (1) Take raw materials according to the following weight ratio: 50% of water, 30% of magnesium chloride, 3% of potassium chloride, 2% of sodium chloride, and 15% of bentonite.

[0034] Among them: magnesium chloride refers to anhydrous magnesium chloride; potassium chloride refers to potassium fertilizer with a potassium chloride content of more than 95%; sodium chloride refers to rock salt for industrial use; bentonite refers to bentonite for drilling mud.

[0035] (2) Add water into the stirring tank, then add magnesium chloride, and stir to completely dissolve the magnesium chloride.

[0036] (3) Add potassium chloride and sodium chloride in sequence in the stirring tank, and stir to dissolve them.

[0037] (4) Add bentonite in the mixing tank and stir evenly.

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PUM

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Abstract

The invention relates to a preparation method of potassium magnesium salt mine drilling fluid, which includes the following steps: (1) weighing and taking raw materials according to the following proportion by weight 50-70% of water, 20-30% of magnesium chloride, 0.1-4% of potassium chloride, 0.1-3% of sodium chloride, 4-15% of bentonite and 0-1% of carboxymethylcellulose; (2) adding water into a stirring tank, adding magnesium chloride, and stirring to enable the magnesium chloride to be dissolved completely; (3) adding potassium chloride and sodium chloride sequentially into the stirring tank and stirring to enable the potassium chloride and sodium chloride to be dissolved; and (4) adding the bentonite and the carboxymethylcellulose into the stirring tank, stirring evenly, and obtaining the potassium magnesium salt mine drilling fluid. The preparation method is simple in process, low in cost and capable of effectively avoiding corrosion of a wall of a well. Compared with the prior art, salt mine core extracting rate can be effectively improved, and an improving effect of core extracting rate for a sylvine layer, especially for a carnallite mineral layer is remarkable.

Description

technical field [0001] The invention relates to the technical field of salt mine exploration, in particular to a preparation method of drilling fluid for potassium-magnesium salt mines. Background technique [0002] Drilling fluid technology is the key technology for the success of drilling in salt deposits. There are many successful precedents in China for drilling protection holes with potassium chloride and sodium chloride, but there is no experience for drilling protection holes with carnallite (potassium-magnesium salt mine). The traditional salt mine drilling fluid is a saturated brine solution, which can prevent fresh water from dissolving the salt mine wall and core, but when drilling into the carnallite (potassium, magnesium chloride) layer, regardless of the Saturated brine solution or saturated potassium salt solution cannot effectively prevent the drilling fluid from dissolving the wall and core of the carnallite mine, and often the core cannot be mined or the co...

Claims

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Application Information

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IPC IPC(8): C09K8/16
Inventor 马海州山发寿曾金波
Owner QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI
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