Preparation method of N (nitrogen)-enriched activated carbon electrode
An activated carbon and electrode technology, which is applied in the field of preparation of N-rich activated carbon electrodes, can solve the problems of low yield, high energy consumption, and limited commercialization process.
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[0004] The present invention is realized according to the following process:
[0005] 1. Use waste fiberboard as raw material (containing about 10% urea-formaldehyde glue), put it into a carbonization furnace, heat up at a rate of 10°C / min, rise from room temperature to 500°C, and carbonize for one hour;
[0006] 2. Take out the carbonized material, prepare it into 40-60 mesh powder, and fully impregnate the carbonized material with KOH (KOH is made into a 50% solution in advance) at a ratio of 3:1 for 16 hours. Put it in an activation furnace and activate it at 800°C for 1 hour to prepare activated carbon. (Specific surface area: 1658m 2 / g; iodine value: 1413mg / g, methylene blue: 13.4mL / 0.1g, pore volume: 0.93cm 3 / g, micropore volume: 0.63cm 3 / g)
[0007] 3. Boil the prepared activated carbon with 0.5M hydrochloric acid for 0.5 hour, then wash with distilled water until neutral, put into oven and dry to obtain activated carbon (the performance of activated carbon is ch...
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