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Quality control and detection method for sea dragon and gecko oral liquid

A technology of Hailong gecko oral liquid and gecko oral liquid, which is applied in the field of quality control and testing of Hailong gecko oral liquid, can solve the problems of comprehensive control and testing, inability to guarantee the quality of medicines, and few testing items, so as to increase the number of people with indications, Increase the effect of high-performance liquid chromatography to determine content and advanced detection methods

Active Publication Date: 2011-10-19
山东宏济堂制药集团股份有限公司
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  • Application Information

AI Technical Summary

Problems solved by technology

In the original standard, only the TLC identification of the medicinal materials ginseng and scutellaria baicalensis, because the original standard has few testing items and a single method, it cannot guarantee the comprehensive control and testing of the quality of the drug

Method used

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  • Quality control and detection method for sea dragon and gecko oral liquid
  • Quality control and detection method for sea dragon and gecko oral liquid
  • Quality control and detection method for sea dragon and gecko oral liquid

Examples

Experimental program
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Effect test

Embodiment 1

[0035] Take sea dragon 39.1g, gecko 0.73g, ginseng 4.68g, sheep whip 4.68g, sheep outer kidney 4.68g, scutellaria 4.68g, rehmannia glutinosa 3.1g, dodder seed 3.1g, polygonum multiflorum 3.1g, rehmannia glutinosa 3.1g, tangerine peel 3.1g, angelica 1.56g, Astragalus 4.68g, Actinolite 1.56g, Lotus hair 1.56g, Licorice 1.56g, Chuanxiong 1.56g, Alisma 1.56g, Cynomorium 1.56g, Cardamom 1.56g, Agarwood 1.56g, Velvet 1.56g, Chinese wolfberry 1.56g, Cistanche 0.78g, Epimedium (Lamb Oil) 1.56g, Cinnamon 1.56g, Leek Seed 1.56g, Cnidium Seed 1.56g, Chinese Pepper 0.31g Twenty-Nine Flavor Ingredients Decoction twice in water, 2 hours each time , Combine the decoction and concentrate it at 80°C to a clear paste with a relative density of 1.04~1.06, add twice the amount of ethanol, refrigerate for 12 hours, filter, concentrate, add water, refrigerate, filter, and add appropriate amount of benzoic acid to the filtrate to dissolve. Use 8% sodium hydroxide to adjust the pH value of 4.6 to 4.8,...

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Abstract

The invention discloses a quality control and detection method for a sea dragon and gecko oral liquid. In the quality control and detection method, on the basis of the original detection standard, a thin-layer chromatography detection method for dried tangerine or orange peel and astragalus root in the prescription of the sea dragon and gecko oral liquid is added, a thin-layer chromatography for ginseng and the astragalus root is improved, and a high performance liquid chromatography for measuring the content of epimedim herb of in the prescription is added. The detection project designed by the invention is reasonable; and the detection method provided by the invention has the advantages of advancement and good accuracy and repeatability, is used for carrying out the quality control on the sea dragon and gecko oral liquid, and can carry out the comprehensive quality control on the sea dragon and gecko oral liquid to ensure the stability and uniformity of product quality.

Description

Technical field [0001] The invention discloses a quality control and detection method of Hailong gecko oral liquid with the effects of warming kidney and strengthening yang and nourishing essence and blood. Background technique [0002] "Hailong Gecko Oral Liquid" functions and indications: warming the kidney and strengthening yang, replenishing essence and blood. Used for sore waist and feet, pale complexion, impotence and spermatorrhea, cold uterus, infertility, and dizziness. [0003] The original test standard of "Hailong Gecko Oral Liquid" is included in the 13th volume of the Pharmaceutical Standards of the Ministry of Health of the People's Republic of China on Prescriptions of Traditional Chinese Medicine. In the original standard, only the medicinal materials ginseng and scutellaria baicalensis were identified by thin layer chromatography. Because the original standard had few test items and a single method, it could not guarantee the comprehensive control and testing of ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/9064G01N30/36G01N30/90A61P1/14A61P15/08A61K33/26A61K35/32A61K35/48A61K35/56A61K35/583A61K35/60
Inventor 李樱刘圣梅姜广玲秦秀玲
Owner 山东宏济堂制药集团股份有限公司
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