Method for preparing miniature thermocouple probe of scanning thermal microscopy
A technology of scanning thermal microscope and thermocouple, which is applied in the field of nanometer sensors and nanometers to achieve the effect of simple process and low equipment dependence
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[0035] The present invention will be further described below through specific embodiments in conjunction with the accompanying drawings, but the present invention is not limited in any way.
[0036] In this example, the commercialized AFM contact mode silicon nitride tip is used, and titanium and palladium are selected as the two metal layer materials of the thermocouple to make a miniature thermocouple probe suitable for the cantilever mount of the VEECO D-3100 AFM instrument. ,Specific steps are as follows.
[0037] (a) Select the AFM cantilever needle tip (model DNP-20, VEECO, USA) that is conveniently available on the market ( figure 1 ), and a miniature thermocouple was prepared on the tip of one of the V-shaped cantilever needles. figure 2 It is a schematic diagram of the process of making a thermocouple. In order to simplify the expression, only one of the four needle points is actually drawn (such as figure 2 shown in a). In steps a and c, the metals used are sele...
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