Method for coagulating coal-bed gas produced water
A treatment method and technology of produced water, applied in the field of water treatment, can solve problems such as the treatment and utilization technology of coalbed methane produced water, and achieve the goal of promoting harmless treatment and resource utilization, reducing treatment load and avoiding environmental pollution Effect
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Embodiment 1
[0022] Example 1: Inorganic coagulants and organic flocculants were selected from commercially available solid polyaluminum chloride (aluminum oxide content 29%) and 40% polydimethyldiallylammonium chloride aqueous solution;
[0023] a. Compounding of polyaluminum chloride and polydimethyldiallylammonium chloride: ① At 20°C, under the conditions of stirring speed of 200r / m and stirring time of 0.5h, 5kg of solid polychlorinated Aluminum chloride is dissolved to form 50kg of polyaluminum chloride aqueous solution; ② Directly use 100g of 40% polydimethyldiallylammonium chloride aqueous solution; ③ At 20°C, add ② solution to ① solution, and the Stir for 1.5 hours under the same conditions to prepare a stable compound coagulant, wherein the mass ratio of the organic flocculant to the alumina in the inorganic coagulant is about 1:15;
[0024] b. The produced water of coalbed methane flows out after initial settlement in the pretreatment tank, and a drug dissolving box is installed ...
Embodiment 2
[0029]Example 2: commercially available solid aluminum sulfate (alumina content 15.6%) and polyacrylamide were selected as the inorganic coagulant and the organic flocculant respectively;
[0030] a. The coalbed methane produced water flows out after the initial settlement of the pretreatment tank. Set up two dissolving boxes at the outlet of the pretreatment tank to stir and dissolve solid aluminum sulfate and polyacrylamide respectively. The diluted concentrations are 15% and 0.5% respectively ;
[0031] b. Dosing diluted polyaluminum chloride and polydimethyldiallyl ammonium chloride solution sequentially through a metering pump or a flow meter, the control dosage is 100mg / L and 2mg / L respectively, and the dosage interval is 1.2min;
[0032] c. After the coalbed methane produced water after dosing has stayed in the flocculation and sedimentation tank for 1 hour, the water quality analysis results are shown in Table 2, and the effluent can reach the discharge standard.
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Embodiment 3
[0036] Example 3: The inorganic coagulant is selected from self-made liquid polyaluminum chloride (aluminum oxide content 10%), and the organic coagulant is selected from the combination of polyacrylamide and 40% polydimethyldiallylammonium chloride aqueous solution (mass ratio 1:250), the coagulation aid is commercially available potassium permanganate;
[0037] a. Compounding of polyaluminum chloride, polyacrylamide, and polydimethyldiallyl ammonium chloride: ① directly use 50 kg of polyaluminum chloride liquid; Under the condition of stirring time of 1h, mix 1g of polyacrylamide and 250g of 40% polydimethyldiallylammonium chloride aqueous solution (mass ratio 1:250), and then, under the condition of ultrasonic frequency of 40kHz, accelerate Dissolve for 0.5h to form a 40% flocculant aqueous solution; ③At 25°C, add ②solution to ①solution and stir for 1h at a speed of 300r / m to obtain a stable compound coagulant agent, in which organic flocculation The mass ratio of aluminum...
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