Thiophene adsorbents and application thereof
A technology of adsorbent and thiophene, which is applied to the purification treatment agent for removing thiophene in aqueous solution and its treatment field, can solve the problems of unsatisfactory treatment effect, complicated process and high treatment cost, and achieves significant practical value, strong adsorption effect, and solution Effects of pollution problems
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Embodiment 1
[0017] Accurately weigh 23.800g of Zn(NO 3 ) 2 .6H 2 O, 15.005g of Al(NO 3 ) 3 .9H 2 O, and 23.070g of sodium dodecyl sulfate (SDS) were put in a beaker, added 400mL of distilled water, stirred to make it completely dissolved, and then transferred to a 1000mL three-necked flask. 2M NaOH solution was added dropwise to maintain the pH at 7, the temperature was controlled at 30° C., and the crystallization time was 12 h. Finally, centrifuge filtration and vacuum drying to obtain the desired product, which is denoted as SDS-ZnAl-LDH.
[0018] In a 1000mL reaction vessel, measure 500mL of a solution with a thiophene concentration of 800mg / L, keep the temperature of the water bath at 25°C, pH=6.33, add 1.2g of SDS-Zn 2 al 1 -LDH, stirred for 6 hours, extracted a certain amount of reaction solution, filtered to obtain the upper clear night, measured the remaining content of thiophene, and calculated the adsorption rate to be 74.74%.
Embodiment 2
[0020] Accurately weigh 23.800g Zn(NO 3 ) 2 .6H 2 O and 15.005g Al(NO 3 ) 3 .9H 2 Put O in a beaker, add 200mL deionized water, stir to dissolve it completely, and record it as solution A; accurately weigh 8.479g Na 2 CO 3 Put 7.680g NaOH in a beaker, add 200mL deionized water, stir to dissolve completely, and record it as solution B. Mix A and B solutions quickly in a rotating liquid film nucleation reactor, vigorously circulate and stir for 2 minutes, then crystallize the slurry at 80°C for 24 hours, and finally centrifugally filter and dry to obtain the desired product, which is designated as ZnAL-CO 3 -LDH.
[0021] In a 1000mL reaction vessel, measure 500mL of a solution with a thiophene concentration of 800mg / L, keep the temperature of the water bath at 25°C, pH=6.33, and add 1.2g of Zn 2 AL 1 -CO 3 -LDH, stirred for 5 hours, extracted a certain amount of reaction solution, filtered to obtain the upper clear night, measured the remaining content of thiophene, a...
Embodiment 3
[0023] In a 100mL Erlenmeyer flask, measure 100mL of a solution with a thiophene concentration of 800mg / L, control the temperature at 25°C, and pH=6.33, add 0.4g of the SDS-ZnAl-LDH prepared in Example 1, stir for 5h, and filter to obtain the upper layer In the clear night, the remaining content of thiophene was measured, and the adsorption rate was calculated to be 82.84%.
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