Method for preparing peroxysulfuric acid by sonoelectrochemical method
A technology of ultrasonic electrochemistry and monosulfuric acid, applied in the electrolysis process, electrolysis components, electrolysis organic production and other directions, can solve the problems such as no successful reports of synthesis, shorten the reaction time, reduce the concentration polarization, and improve the current efficiency Effect
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Embodiment 1
[0014] Add sulfuric acid solution with a concentration of 20% into the electrolytic cell, pure platinum is the anode, the cathode is the lead plate, the sulfonic anion membrane separates the negative and positive areas, ultrasonic waves are added to the bottom of the electrolytic cell, the electrolytic voltage is 3V, and the current density is 1500A / m 2 , the ultrasonic frequency is 20kHz, and the ultrasonic sound intensity is 10W / m 2 , the reaction temperature is 0°C, ultrasonic electrolysis is performed for 4 hours, and the concentration of the prepared oxidant peroxymonosulfuric acid is 0.9 mol / L.
Embodiment 2
[0016] Add sulfuric acid solution with a concentration of 30% into the electrolytic cell, pure platinum is the anode, the cathode is the lead plate, the sulfonic anion membrane separates the negative and positive areas, the electrolytic voltage is 5V, and the current density is 2500A / m 2 , add ultrasonic waves at the bottom of the electrolytic tank, the ultrasonic frequency is 60kHz, and the ultrasonic sound intensity is 5W / cm 2 , the reaction temperature is 20 DEG C, ultrasonic electrolysis is carried out for 3 hours, and the concentration of the prepared oxidant peroxymonosulfuric acid is 0.95 mol / L.
Embodiment 3
[0018] Add sulfuric acid solution with a concentration of 45% into the electrolytic cell, pure platinum is the anode, the cathode is the lead plate, the sulfonic anion membrane separates the negative and positive areas, the electrolysis voltage is 6V, and the current density is 5000A / m 2 , add ultrasonic waves at the bottom of the electrolytic tank, the ultrasonic frequency is 100kHz, and the ultrasonic sound intensity is 20W / cm 2 , the reaction temperature is 40 DEG C, ultrasonic electrolysis for 2 hours, the concentration of the prepared oxidant peroxymonosulfuric acid is 1mol / L.
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