Organosilicon concrete protectant and preparation method thereof
A technology for concrete and protective agent, applied in the field of silicone concrete protective agent and its preparation, can solve the problems of bubbling of protective agent coating, small molecular structure, peeling off, etc. cracked effect
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Embodiment 1
[0036] 13.5 kilograms of concentrated hydrochloric acid (mass fraction 35%) and 32.4 kilograms of distilled water were mixed uniformly to make a mixed solution of concentrated hydrochloric acid and distilled water for use. In the reactor with heating, stirring and reflux devices, add 6.8 kg of methyl propyl diethoxysilane, 13.5 kg of n-propyl triethoxy, 13.5 kg of long chain alkyl triethoxy silane, 6.8 kilograms of tetraethoxysilane and 13.5 kilograms of ethanol are heated up. When the temperature rises to 75°C, slowly drop the mixture of concentrated hydrochloric acid and distilled water into the reactor, stir rapidly at a speed of 150 rpm, and react for 6 to 8 hours; after the stirring reaction is completed, evaporate the solvent under reduced pressure The ethanol and the ethanol produced by the reaction are cooled to below 40° C. with tap water, and then subjected to suction filtration to obtain an alkylsilane oligomer.
[0037] Add 15 kg of alkylsilane oligomers, 3 kg of ...
Embodiment 2
[0039] 13.5 kilograms of concentrated hydrochloric acid (mass fraction 35%) and 32.4 kilograms of distilled water were mixed uniformly to make a mixed solution of concentrated hydrochloric acid and distilled water for use. In the reactor with heating, stirring and reflux devices, add 6.8 kg of methyl propyl diethoxysilane, 13.5 kg of n-propyl triethoxy, 13.5 kg of long chain alkyl triethoxy silane, 6.8 kilograms of tetraethoxysilane and 13.5 kilograms of ethanol are heated and heated; when the temperature rises to 75 ° C, the mixed solution of concentrated hydrochloric acid and distilled water is slowly added dropwise to the reactor, and the speed is stirred at 150 rpm. 6-8 hours; after the stirring reaction is completed, the solvent ethanol and the ethanol produced by the reaction are evaporated under reduced pressure, cooled to below 40°C with tap water, and then subjected to suction filtration to obtain an alkylsilane oligomer.
[0040] Add 22 kg of alkylsilane oligomers, 6...
Embodiment 3
[0042] 13.5 kilograms of concentrated hydrochloric acid (mass fraction 35%) and 32.4 kilograms of distilled water were mixed uniformly to make a mixed solution of concentrated hydrochloric acid and distilled water for use. In the reactor with heating, stirring and reflux devices, add 6.8 kg of methyl propyl diethoxysilane, 13.5 kg of n-propyl triethoxy, 13.5 kg of long chain alkyl triethoxy silane, 6.8 kilograms of tetraethoxysilane and 13.5 kilograms of ethanol are heated and heated; when the temperature rises to 75 ° C, the mixed solution of concentrated hydrochloric acid and distilled water is slowly added dropwise to the reactor, and the speed is stirred at 150 rpm. 6-8 hours; after the stirring reaction is completed, the solvent ethanol and the ethanol produced by the reaction are evaporated under reduced pressure, cooled to below 40°C with tap water, and then subjected to suction filtration to obtain an alkylsilane oligomer.
[0043] Add 20 kg of alkylsilane oligomers, 5 k...
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