Method for preparing microcapsule emulsion used for novel heat-preserving and sound-insulating building coating
A technology for thermal insulation and sound insulation and architectural coatings, which is applied in the directions of microcapsule preparation, microsphere preparation, coating, etc., can solve the problems of lack of thermal insulation and sound insulation performance, poor thermal insulation and sound insulation effect, and high construction requirements, so as to increase elasticity and transmit energy. Insulation and sound insulation, economical effect
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Embodiment 1
[0029] Example 1 Microcapsule emulsion formula core material for new thermal insulation and sound insulation architectural coatings: air, orifice diameter: 1.6 microns, pressure: 3000-3200 Pa, continue to flow for 45 minutes; wall material: melamine 15g, emulsifier: styrene horsedot Toric anhydride 25g, formaldehyde 30ml, ethanol 30ml
Embodiment 2
[0030] Example 2 The formula of microcapsule emulsion for new thermal insulation and sound-proof architectural coatings Core material: carbon dioxide, orifice diameter: 1.6 microns, pressure: 3000-3200 Pa, continue to flow for 45 minutes; wall material: melamine 15g, emulsifier: styrene horsedot Toric anhydride 25g, formaldehyde 30ml, ethanol 30ml
Embodiment 3
[0031] Embodiment 3 The preparation of microcapsule emulsion for novel thermal insulation and sound insulation architectural coating:
[0032] (1) Polymer: Take 30g melamine + 60ml (36%) formaldehyde + 20ml water, slowly heat up to 65°C until the solution is clear, add 60ml ethanol and continue to stir for 10 minutes, then set aside for later use.
[0033] (2) Dissolution of emulsifier: Take 40g of styrene maleic anhydride, adjust the pH to 12 in 100ml of water, slowly heat up to 95°C, and adjust the pH while adding styrene maleic anhydride until dissolved. Adjust PH=7~10 and set aside for later use.
[0034] (3) Sharp hole forming bubbles: take 70ml of emulsifier solution, adjust pH to about 4.5, and ventilate for 45 minutes under stirring at 60°C.
[0035] (4) Polycondensation into capsules: add 45 ml of prepolymer to the above solution for 30 minutes, heat up to 80° C. and stir for 2 hours.
[0036] (5) Discharging: Cool the above solution to room temperature, adjust the ...
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