Method for extracting proanthocyanidin from pine bark by taking water as solvent
A technology of proanthocyanidins and pine bark, applied in the direction of organic chemistry, etc., can solve the problems of poor product safety, high production cost, complicated extraction process, etc., and achieve the effects of less loss, no chemical residue, and high extraction efficiency.
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Embodiment 1
[0022] Weigh 100g of clean, non-rotten and moldy pine bark, crush it to 60 mesh, add 1000mL of distilled water, and ultrasonically extract for 30min under the conditions of ultrasonic power 100W, frequency 20KHz, and temperature 50°C, repeat the extraction once, and combine The leaching solution was centrifuged for 20 minutes at 4000 rpm for 2 times to obtain a clarified leaching solution. The clarified extract is suction-filtered with a 0.45 μm microporous membrane to obtain a microfiltration permeate. The microfiltration permeate was ultrafiltered with a hollow fiber ultrafiltration membrane with a molecular weight cut-off of 100,000 Daltons. At room temperature, the reflux valve was adjusted to control the pressure to 0.1Mpa, and the ultrafiltration permeate was collected. The ultrafiltration permeate was concentrated with a roll-type nanofiltration membrane with a molecular weight cut-off of 200 Daltons. At room temperature, the reflux valve was adjusted to control the pre...
Embodiment 2
[0024]Weigh 10kg of clean, non-rotten and moldy pine bark, crush it to 40 mesh, add 100L deionized water, and ultrasonically extract for 40min under the conditions of ultrasonic power 1000W, frequency 40KHz, and temperature 45°C, and repeat the extraction once , combine the 2 extracts, and use a centrifuge for solid-liquid separation to remove solid impurities to obtain a clarified extract. The clarified extract is sent to the microfiltration device through a booster pump, and microfiltration is carried out with a 0.5μm tubular ceramic microporous filter membrane. The temperature of the feed liquid is controlled at about 35°C, and the return valve is adjusted to control the pressure to 0.6Mpa. liquid. The microfiltration permeate is sent to the ultrafiltration device through a booster pump, and ultrafiltration is performed with a hollow fiber ultrafiltration membrane with a molecular weight cut-off of 100,000 Daltons. The temperature of the feed liquid is controlled at about 3...
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