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Production method of large-size graphite electrode

A graphite electrode and production method technology, applied in the field of large-scale graphite electrode production, to achieve the effects of low impurity content, production cost saving, and unit consumption reduction

Inactive Publication Date: 2012-08-29
JIEXIU JUYUAN & COALY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the shortcomings of carbon electrodes caused by various defects in industrial silicon smelting, the invention provides a production method of large-scale graphite electrodes, which solves the problems existing in the current production of graphite electrodes with a diameter greater than 600mm, and can produce ultra-high-power electrodes with a diameter of 960mm. graphite electrode

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Component distribution ratio (weight ratio): 76% calcined petroleum coke, 24% modified pitch; among them, calcined petroleum coke according to the weight percentage of particle size distribution: 4% for Φ>12mm pellets; 10% for Φ8-12mm pellets; Φ4-8mm granular material 15%; Φ2-4mm granular material 13%; Φ≤0.075mm powder 30%; Φ0.075-2mm filler 4%; the coking value of the modified asphalt is above 55%, The softening point is 95-100°C; after batching according to the above ratio, it is produced by conventional technology, wherein the kneading temperature is 160°C; the lumpiness of the paste is less than 40mm when molded.

Embodiment 2

[0015] Component distribution ratio (weight ratio): 77% calcined petroleum coke, 23% modified pitch; among them, calcined petroleum coke according to the weight percentage of particle size distribution: 2% for Φ>12mm pellets; 8% for Φ8-12mm pellets; Φ4-8mm granular material 13%; Φ2-4mm granular material 11%; Φ≤0.075mm powder 32%; Φ0.075-2mm filler 11%; the coking value of the modified asphalt is above 55%, The softening point is 95-100°C; after batching according to the above ratio, it is produced by conventional technology, wherein the kneading temperature is 165°C; the lumpiness of the paste is less than 40mm when molded.

Embodiment 3

[0017] Component distribution ratio (weight ratio): 79% calcined petroleum coke, 21% modified asphalt; Among them, the weight percentage of calcined petroleum coke according to particle size distribution is: 6% of Φ8-12mm granular material; 17% of Φ4-8mm granular material; Φ2-4mm pellets 9%; Φ≤0.075mm powder 32%; Φ0.075-2mm filler 15%; Φ0.5-2mm particle size 7.5%, Φ0.075-0.5mm 7.5% . The coking value of the modified asphalt is above 55%, and the softening point is 95-100°C; after the above-mentioned ratio of compounding, it is produced by conventional technology, wherein the kneading temperature is 163°C; the lumpiness of the paste is less than 40mm when molded.

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Abstract

The invention relates to a production method of a large-size graphite electrode which comprises the components in percentage by weight: 76-79 percent of calcined petroleum coke, 21-24 percent of medium-high temperature modified asphalt and the balance of filling material with the diameter of 0.075-2 mm, wherein the calcined petroleum coke comprises the following components in percentage by weight: not more than 4 percent of granules with the diameter of more than 12 mm, 6-10 percent of granules with the diameter of 8-13 mm, 13-17 percent of granules with the diameter of 4-8 mm, 9-13 percent of granules with the diameter of 2-4 mm and 30-32 percent of powder with the diameter of not more than 0.075 mm according to the particle size distribution; and the coking value of the modified asphalt is over 55 percent and the softening point is 95-100 DEG C. After the raw materials are mixed according to the proportion, the large-size graphite electrode is produced by adopting a conventional process, wherein the mixing temperature is 160-165 DEG C and the thicker lumpiness during the die-filling is less than 40 mm. A huge-size electrode with the diameter of over 960 mm can be produced by adopting the production method of the large-size graphite electrode; meanwhile, the electrode has low resistivity and good conduction property and can bear strong current, thereby enabling the unit consumption and the electricity consumption to be greatly lowered and saving the production cost.

Description

technical field [0001] The invention relates to a production method of electrodes heated by electric discharge, in particular to a production method of graphite electrodes used in electric furnace smelting or industrial silicon electric heating equipment. Background technique [0002] An electrode is a cylindrical object, an important part of an electric furnace for smelting industrial silicon, and a part of a short network. Rely on the electrode to send the low-voltage and high-current delivered by the furnace transformer to the furnace, and through the arc at the end of the electrode, the resistance of the charge and the melt, the electric energy is converted into heat energy for high-temperature smelting. Therefore, in order to keep the electrode in good and stable operation and reduce the occurrence of electrode accidents as much as possible, the electrode needs the following requirements: 1) It has good conductivity, moderate resistivity, and matches the electrical para...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/622C04B35/532
Inventor 高峰屹渠果明
Owner JIEXIU JUYUAN & COALY
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