Battery electrode paste compound containing modified maleimide
A technology of maleimide and bismaleimide, applied in the field of electrode slurry composition of lithium battery, can solve problems such as sedimentation
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Synthetic example 1
[0032] Synthesis Example 1: Preparation of Modified Bismaleimide Dispersant
[0033] The reactants N, N'-4,4'-diphenylmethane-bismaleimide and barbituric acid (molar ratio 10:1) were placed in the reaction vessel, and then the propenyl carbonate solvent was added to the reaction In the container, the weight ratio of the reactant to the propylene carbonate solvent is 20:80. After mixing, the mixture was heated to 130° C. for 3 hours to obtain a modified maleimide dispersant.
preparation example 1
[0034] Preparation Example 1: Preparation of Positive Plate Slurry
[0035] 1820 grams of lithium cobalt oxide (LiCoO 2 ), 120 grams of KS4, 60 grams of polyvinyl difluoride (PVDF) and 850 grams of N-methylpyrrolidone were placed in a three-dimensional space mixer (3D Mixer). Next, the modified maleimide obtained in Synthesis Example 1 was added into the three-dimensional space mixer (3D Mixer) in an amount of 0.4% by weight of the total solid content of the slurry. Finally, the quantitative standard was added and mixed with the beads and mixed for 2.5 hours, and the mixture was poured out, and the beads were filtered to obtain the slurry sample 1 of the positive electrode.
preparation example 2
[0036] Preparation Example 2: Preparation of Positive Plate Slurry (Control Group)
[0037] 1820 grams of lithium cobalt oxide (LiCoO 2 ), 120 grams of KS4, 60 grams of polyvinyl difluoride (PVDF) and 850 grams of N-methylpyrrolidone were placed in a three-dimensional space mixer (3D Mixer). Next, add the quantitative standard and mix the beads and mix for 2.5 hours, pour out the mixture, filter the beads, and obtain the slurry sample 2 of the positive electrode.
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