Walnut green husk plant miticide and preparation method thereof
A technology of walnut green peel and acaricide, applied in the directions of botanical equipment and methods, acaricides, plant growth regulators, etc. Efficient, beneficial to industrial production, simple and easy to extract
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Embodiment 1
[0062] Wash the green walnut skin, dry it in the shade in a ventilated place, or dry it at 20-45°C, grind it and pass it through a 40-60 mesh sieve. Put the pulverized plant powder into a multifunctional extraction tank, extract with petroleum ether (40-90° C.) or chloroform with 5 times the volume of the plant powder, and collect the chloroform or petroleum ether extract. Take 15kg of the extract, add 70kg of toluene or xylene into a mixing kettle with a stirrer and a thermometer, mix for 1.5 hours at 50°C, add 1kg of Tween (polysorbate), 0.5kg of 6-vinyldecanal, Sodium lauryl sulfate 2kg, benzylphenol polyoxyethylene ether 0.5kg, mix uniformly, obtain walnut green bark extract 16.9% acaricide emulsifiable concentrate.
Embodiment 2
[0064] Wash the green walnut skin, dry it in the shade in a ventilated place, or dry it at 45°C, grind it and pass it through a 60-mesh sieve. Put the pulverized plant powder into a multifunctional extraction tank, extract with 4 times the volume of chloroform, and collect the chloroform extract. Take 10kg of the extract, add 60kg of toluene or xylene into a mixing kettle with a stirrer and a thermometer, mix for 3 hours at 60°C, add 1kg of polyethylene glycol, 1kg of tea saponin, p-octylphenol polyoxygen Vinyl ether 3kg, azone 1kg, mix uniformly, obtain walnut green husk extract 13.2% acaricide emulsifiable concentrate.
Embodiment 3
[0065] Embodiment 3: Preparation of walnut green husk extract
[0066] Adopt multifunctional extracting tank, the volume ratio of the powder of walnut green skin and organic solvent ethanol is 1: 2, 1: 3 or 1: 4, soak in warm or cold for 8, 10, 12, 18 or 24 hours, filter, dry, Get walnut green bark extract.
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