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Electrochemistry test method used for rotary type single-phase flow erosion testing

A test method, electrochemical technology, applied in the direction of measuring devices, scientific instruments, weather resistance/light resistance/corrosion resistance, etc., can solve the problems that the experimental results are difficult to promote engineering applications, the test time of related equipment is long, and the mechanism is not deep enough.

Inactive Publication Date: 2009-07-22
ZHEJIANG SCI-TECH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] (1) At present, the mechanism of erosion test in my country is not deep enough, and the relevant equipment test takes a long time, and the experimental results are difficult to promote engineering applications
[0007] (2) The test method is single; the erosion test of scholars at home and abroad usually puts the metal specimen into the corrosive medium, by increasing the flow rate or rotating speed, and statically testing the loss of metal by weighing, it is impossible to realize the fluid erosion damage. Study on Transient Characteristics of Critical Value

Method used

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  • Electrochemistry test method used for rotary type single-phase flow erosion testing
  • Electrochemistry test method used for rotary type single-phase flow erosion testing

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Embodiment Construction

[0029] The present invention will be further described below in conjunction with drawings and embodiments.

[0030] like figure 1 As shown, the rotary single-phase flow erosion test device includes a working electrode 12, a Lujin capillary 9, a salt bridge 8, a reference electrode 7, an auxiliary electrode 13, a copper ring-carbon brush 4, a potentiostat 11, and an industrial computer 6 . The transmission shaft 2 is equipped with a rotating disk 10, the workpiece to be measured is used as a working electrode, and its outer surface is flush with the inner wall of the upper liquid container 3. The working electrode 12 and the auxiliary electrode 13 coated with a layer of stainless steel or platinum on the side of the rotating disk On the same horizontal plane; the sides of the rotating disc are respectively opened at 0°, 90°, 180°, and 270°, and the wires pass through the holes of 0°, 90°, 180°, and 270° respectively and meet at the rotating disc One end of the central hole of...

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Abstract

The invention discloses an electrochemical test method applied to a rotary single-phase flow erosion test. Make the working electrode of the test piece and install it on the test device, adjust the distance between the working, reference and auxiliary electrodes; add the corrosive solution to be tested from the feeding port on the top of the container and be 75mm higher than the auxiliary electrode; The electrochemical method of adding passivation potential to the working electrode pre-corrodes the working electrode until the current becomes smaller and tends to be stable, so that a uniform and dense corrosion product protective film is formed on the surface of the working electrode; turn on the frequency conversion motor, and use the computer to follow the preset acceleration curve Slowly increase the speed, and observe the current curve of the potentiostat until a sudden change occurs. It is suitable for the experimental research of the critical characteristics or transient characteristics of the erosion damage of the protective film under the coupled action of corrosion and flow. It can simulate the actual working conditions in the industrial environment, and the electrochemical test for real-time detection of the transient characteristics and critical values ​​of material erosion damage method.

Description

technical field [0001] The invention relates to an electrochemical testing method for erosion tests, in particular to an electrochemical testing method applied to rotary single-phase flow erosion tests. Background technique [0002] Fluid pipeline is a special equipment for transporting fluid under certain pressure. It has become one of the five major transportation modes alongside road, railway, water transportation and aviation. Transport of fluid materials. Fluid pipelines are widely used in the national economy, but the erosion failure of the pipeline system by corrosive multiphase flow is obviously localized and sudden, and the safety risk is great. [0003] Corrosion of pipelines will not only cause oil and gas leakage loss due to perforation and waste of materials and manpower due to maintenance, but may also cause fire due to corrosion perforation. Especially for high-pressure gas pipelines, once they rupture, the compressed gas expands rapidly, releasing a large a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N17/02
Inventor 偶国富许根富梁灵鹏
Owner ZHEJIANG SCI-TECH UNIV
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