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Quality Controlling method of Qianlieshule preparation

A quality control method and technology of Qianlieshu, applied in the field of quality control of traditional Chinese medicine preparations, can solve problems such as affecting product production and quality assurance, and failing to effectively control the quality of Qianlieshu preparations.

Inactive Publication Date: 2006-08-16
JIANGXI HUIREN PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, the existing quality control methods cannot effectively control the quality of Qianlieshule preparations, which will affect the production and quality assurance of products

Method used

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  • Quality Controlling method of Qianlieshule preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0147] The quality control of embodiment 1 Qianlieshule mixture

[0148] The quality control method of the present invention comprises the following steps:

[0149] The observation of traits, the steps are:

[0150] 【Properties】This product is a dark brown or black liquid with a small amount of precipitation; the taste is slightly bitter.

[0151] Content identification, the steps are:

[0152] [Identification] (1) Take 10ml of this product, put it in a stoppered test tube, shake vigorously for 1 minute, and produce stable and persistent foam.

[0153] (2) Take 4ml of this product, put it in a test tube, add 4-5 drops of 0.5% ninhydrin ethanol solution, mix well, put it in a boiling water bath and heat it for several minutes, and it will appear purple.

[0154] (3) Take 10ml of this product, evaporate to dryness in a water bath, add 10ml of absolute ethanol, ultrasonically treat for 10 minutes, filter, take 2ml of the filtrate, wave it to 1ml in a water bath, add appropriat...

Embodiment 2

[0168] Embodiment 2 Qianlieshule mixture

[0169] The prescription consists of:

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Abstract

A method for controlling quality of qianlieshu preparation utilizes thin layer chromatography to carry out identification and utilizes spectrophotomentry to carry out content determination for ensuring produce quality.

Description

Technical field: [0001] The invention relates to a quality control method for traditional Chinese medicine preparations, in particular to a quality control method for Qianlieshule preparations. Background technique: [0002] Qianlie Shule preparation is made by extracting and processing 5 herbs of Epimedium, Astragalus, Pollen, Plantain and Achyranthes bidentata. [0003] Qianlie Shule Granules, recorded in the Ministry of Health Drug Standards Traditional Chinese Medicine Prescriptions Volume 12, page 142. It is a national essential medicine (surgical medicine-prostatic hyperplasia-Yang deficiency and blood stasis syndrome) and a social insurance product (Class B, internal medicine medicine-dampness-dispelling agent-removing stasis and treating stranguria; when it is limited to outpatient use, it will be paid by the basic medical insurance fund according to regulations) , its function cures mainly for invigorating the kidney and replenishing qi, dispelling blood stasis and...

Claims

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Application Information

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IPC IPC(8): G01N33/15G01N30/90G01N30/02G01N30/06G01N1/28
Inventor 薛建国耿炤
Owner JIANGXI HUIREN PHARMA CO LTD
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