Method of fabricating polyurethane foam with micro pores and polishing pad therefrom
A technology of polyurethane foam and polishing pad, applied in the field of polishing pad, can solve the problems of high production cost, damaged processing allowance, performance change, etc., and achieve the effects of reducing processing cost, increasing processing allowance, and increasing selection possibility
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Embodiment approach 1
[0075] Such as figure 2 As shown in the schematic diagram of , 1 part by weight of a hydroxyl-containing silicone-based surfactant (trade name: DC-193, DOW CORNING Co., Ltd.) and 100 parts by weight of an isocyanate-terminated urethane prepolymer Adiprene L-325 were mixed and then reacted with each other at a temperature of 60°C for 2 hours. As a result, the hydroxyl group of the polysiloxane-based surfactant is deactivated and a uniform and stable urethane prepolymer reaction liquid (first component liquid) is obtained. This first component liquid is transferred to an air nucleation type molding machine 100, and then, a non-reactive gas N is injected thereinto using a mass flow meter 104. 2 , while injecting 24 parts by weight of MBCA (relative to 100 parts by weight of isocyanate-terminated urethane prepolymer Adiprene L-325) dissolved at a temperature of 120° C. as a second component liquid therein. Next, the mixture is mixed and stirred by the rotating paddle 108, and p...
Embodiment approach 2-9
[0079] By the same method as Comparative Example 1, by changing the content of surfactant, the amount of poured mixture and the injection amount of non-reactive gas, etc., wherein the composition ratio is shown in Table 1 below, polishing pads were prepared, and these polishing pads were evaluated. The polishing properties of the pad. The evaluation results are shown in Table 2. The polishing pad prepared by Embodiment 2 was inspected by SEM, and it was found that the pores formed thereon were very uniform and fine. (see Figure 4 )
[0080] carbamic acid
Ethyl prepolymerized
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