Burdock inulin and its preparing method
A kind of technology of burdock inulin and inulin, applied in the field of burdock inulin and its preparation
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Embodiment 1
[0038] Take fresh burdock root, wash it with tap water, dry it naturally, cut it into thin slices with uniform size and thickness by hand or with a slicer, dry it in an oven at 60°C, and crush it mechanically to about 40 meshes to become dry burdock powder, which is weighed for later use.
[0039] Extract the burdock powder with 10 times the volume of hot water at a constant temperature of 80°C. Filter after each extraction, use a double-layer filter cloth for initial filtration, and then filter the filtrate with a Buchner funnel to completely separate the residue (burdock residue is used to extract dietary fiber) and extract, and combine the extract. Put the acidified (pH=4) macroporous adsorption resin (3250 resin or resin of other specifications) into a chromatographic column (Φ3.5×50cm or other specifications), equilibrate with deionized water, and extract The liquid flows through the resin bed at a certain flow rate to elute small molecular impurities and decolorize, rece...
Embodiment 2
[0041] Take fresh burdock root, wash it with tap water, dry it naturally, cut it into thin slices with uniform size and thickness manually or with a slicer, oven dry at 50°C, and mechanically crush it to about 40 meshes to become dry burdock powder, which is weighed for later use.
[0042] Extract the burdock powder with 15 times the volume of hot water at a constant temperature of 85°C. Filter after each extraction, use a double-layer filter cloth for initial filtration, and then filter the filtrate with a Buchner funnel to completely separate the residue (burdock residue is used to extract dietary fiber) and extract, and combine the extract. Put the acidified (pH=4) macroporous adsorption resin (3250 resin or resin of other specifications) into a chromatographic column (Φ3.5×50cm or other specifications), equilibrate with deionized water, and extract The liquid flows through the resin bed at a certain flow rate to elute small molecular impurities and decolorize, receive the ...
Embodiment 3
[0044] Take fresh burdock root, wash it with tap water, dry it naturally, cut it into thin slices of uniform size and thickness by hand or with a slicer, dry in an oven at 65°C, and crush it mechanically to about 40 meshes to become dry burdock powder, which is weighed for later use.
[0045] Extract the dried burdock powder at 80°C with 8 times the volume of hot water. Filter after each extraction, use a double-layer filter cloth for initial filtration, and then filter the filtrate with a Buchner funnel to completely separate the residue (burdock residue is used to extract dietary fiber) and extract, and combine the extract. Put the acidified (pH=4) macroporous adsorption resin (3250 resin or resin of other specifications) into a chromatographic column (Φ3.5×50cm or other specifications), equilibrate with deionized water, and extract The liquid flows through the resin bed at a certain flow rate to elute small molecular impurities and decolorize, receive the effluent, and use ...
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