Method for producing micro crystal wax
A technology of microcrystalline wax and hydrogenation method, applied in petroleum wax refining and other directions, can solve the problems of increasing hydrogen consumption, increasing equipment investment and operating costs, reducing the processing capacity of hydrogenation catalysts, etc., so as to reduce hydrogen consumption and equipment investment. and operating costs, the effect of easy long-term stable operation
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Embodiment 1
[0021] The soft microcrystalline wax raw material containing 4.11% oil is used, and the properties are shown in Table 1. Two reactors are used, and the same hydrorefining catalyst is used. The properties of the catalyst are shown in Table 2. Catalyst A.
[0022] The oil-hydrogen mixture heated to a certain temperature first enters the first reaction section, and under the action of the catalyst, by controlling the appropriate reaction conditions, mainly undergoes hydrodesulfurization, denitrogenation, and deoxygenation reactions; the material flowing out of the first reaction section passes through After cooling down, it enters the second reaction section. Under the action of the catalyst, by controlling the appropriate reaction conditions, the aromatic hydrocarbon saturation reaction is mainly carried out; after the material flows out of the second reactor, it is white after gas-liquid separation and vacuum deodorization Soft microcrystalline wax product. The process conditio...
Embodiment 2
[0024]The raw material used in this embodiment is oil-containing 3.06% soft microcrystalline wax raw material (referring to Table 1), and the catalyst is the same as in Example 1, and the loading amount (body) is one reverse: the two reverse is 2: 3, and the process conditions and product properties are respectively See Tables 3 and 4.
Embodiment 3
[0026] The used raw material of this implementation is the soft microcrystalline wax raw material (referring to table 1) that contains oil 2.21%, two bed layers are filled in a reactor, and two bed layers use identical hydrorefining catalyst, and catalyst properties are shown in table 2 Catalyst A, cold hydrogen is pumped between the two beds to reduce the temperature of the material. The process conditions and product quality are shown in Tables 3 and 4, respectively.
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