A kind of rare earth-based infrared heating warm fabric and its preparation method and application
A rare earth-based, infrared technology, applied in the field of textile fabrics, can solve the problems of inconvenient washing and inability to wash with water, and achieve the effect of simple structure and excellent thermal conductivity
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Embodiment 1
[0043] Example 1 Preparation of Gd 0.1 La 0.9 B 6 Powder, including the following steps:
[0044] (1) Press Gd:La:B:Na:SiO 2 The molar ratio is the ratio of 0.1:0.9:6:24:12, respectively weighing Gd 2 (CO 3 ) 3 495g, La 2 (CO 3 ) 3 2060g, B 2 O 3 2089g, Na 552g, SiO 2 720g, all the raw materials were put into the autoclave, 12 moles of hydrogen were introduced, heated to 320°C, and stirred for two hours. The obtained product was extracted with deionized water and separated into layers, the precipitated part was filtered and washed with water for 5 times, and the obtained product was dried at 110° C. for 5 hours. After drying, the product and 6 kg of deionized water were loaded into a sand mill for grinding for 8 hours. After testing, the particle size of the slurry was 500-700 nanometers. The slurry was first spray granulated and dried, and the particle size of the obtained powder was 700 nanometers. -800 nm. The 700-800 nanometer powder is subjected to the sec...
Embodiment 2
[0047] Example 2 Preparation of Ce 0.1 La 0.9 B 6 Powder, as Ce:La:B:Na:SiO 2 The molar ratio is 0.1:0.9:6:24:12, respectively weighing Ce(NO 3 ) 3 326g, La 2 (CO 3 ) 3 2060g, B 2 O 3 2089g, Na 552g, SiO 2 720g, the remaining steps are the same as 1.1 to prepare Gd 0.1 La 0.9 B 6 The steps for powder are the same.
Embodiment 3
[0048] Example 3 Preparation of Sm 0.1 La 0.9 B 6 Powder, according to Sm:La:B:Na:SiO 2 The molar ratio is 0.1:0.9:6:24:12, respectively weigh Sm(NO 3 ) 3 336g, La 2 (CO 3 ) 3 2060g, B 2 O 3 2089g, Na 552g, SiO 2 720g, the remaining steps are the same as 1.1 to prepare Gd 0.1 La 0.9 B 6 The steps for powder are the same.
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