Ultrasonic-assisted supercritical extraction tank and preparation method of Sichuan-style capsanthin oil
An ultrasonic-assisted, extraction tank technology, which is applied in the fields of fat oil/fat refining, edible oil/fat, fat oil/fat production, etc., can solve the problems of decreased spiciness, dark color, and low product quality, so as to promote full contact, The effect of low temperature and high efficiency preparation
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Embodiment 1
[0040] Such as figure 1 Shown:
[0041] The invention provides an ultrasonic-assisted supercritical extraction tank, comprising an extraction tank body, an ultrasonic controller 1, and an ultrasonic generator 2; wherein,
[0042] The bottom and the top of the extraction tank are respectively provided with an inlet and an outlet of supercritical carbon dioxide, and an inlet pipe 3 and an outlet pipe 4 are respectively connected to the outlet and the inlet; There is an upper filter device 5, a plurality of baffles 6, and a lower filter device 7; a heating jacket 8 is provided on the outside of the extraction tank;
[0043] The ultrasonic generator 2 is arranged in the extraction tank; the extraction tank is also connected with a temperature sensor 9 for monitoring the internal temperature of the extraction tank and a pressure gauge 10 for monitoring the pressure;
[0044]The ultrasonic controller 1 is electrically connected with the ultrasonic generator 2;
[0045] The ultras...
Embodiment 2
[0054] A kind of preparation method of Sichuan style capsicum red oil, comprises the steps:
[0055] S1. Raw material pretreatment
[0056] removing impurities from the dried red pepper, cleaning, roasting, and pulverizing to 40 mesh to obtain pepper noodles;
[0057] Baking is baking at a temperature of 135°C for 5 minutes;
[0058] S2. Ultrasonic-assisted supercritical carbon dioxide extraction
[0059] Put the chili powder obtained in step S1 into the ultrasonic-assisted supercritical extraction tank in Example 1, and add an entrainer at the same time; extract at an extraction temperature of 40°C, a fluid extraction pressure of 30MPa, and a carbon dioxide flow rate of 25L / h; extract for 30min Finally, the ultrasonic generator 2 is intermittently turned on for ultrasonic-assisted extraction. The ultrasonic time is 5s each time, and the intermittent time is 9s. The extraction temperature is kept at 40°C, the fluid extraction pressure is 30MPa, and the carbon dioxide flow ra...
Embodiment 3
[0066] A kind of preparation method of Sichuan style capsicum red oil, comprises the steps:
[0067] S1. Raw material pretreatment
[0068] removing impurities from the dried red pepper, cleaning, roasting, and crushing to 60 mesh to obtain pepper noodles;
[0069] Baking is at a temperature of 150°C for 4 minutes;
[0070] S2. Ultrasonic-assisted supercritical carbon dioxide extraction
[0071] Put the chili noodles obtained in step S1 into the ultrasonic-assisted supercritical extraction tank in Example 1, and add an entrainer at the same time; extract at an extraction temperature of 45 ° C, a fluid extraction pressure of 20 MPa, and a carbon dioxide flow rate of 30 L / h; extract for 30 minutes Finally, the ultrasonic generator 2 is intermittently turned on for ultrasonic-assisted extraction, each ultrasonic time is 6s, and the intermittent time is 8s, and the extraction temperature is kept at 45°C, the fluid extraction pressure is 20MPa, and the carbon dioxide flow rate is...
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