Preparation method of seam bonding belt bonding layer material for repairing asphalt pavement
A technology of asphalt pavement and adhesive layer, which is applied in the direction of asphalt material adhesive, adhesive, adhesive type, etc. It can solve the problems of adhesive layer peeling, water entering cracks, and inability to play a repairing role, so as to achieve optimal performance , good adhesive performance, and the effect of widening the applicable temperature range
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Embodiment 1
[0036] (1) Preparation of modifier: Add 0.05mol racemic polylactic acid, 0.055mol DCC and 0.055mol HOBt to tetrahydrofuran, heat to 55°C to dissolve, then add 0.06mol 3-(N-allylamino)propyl base trimethoxysilane, heated to 55 ° C for 8 hours, after the reaction, add water to precipitate, filter with suction, and dry to obtain the modifier;
[0037] (2) Preparation of modified asphalt: Heat 100g of 90# petroleum asphalt to 180°C to completely flow, then add 10g of the modifier prepared above, and transfer it to a high-speed shearing machine for processing, the shearing temperature is 180°C, and the shearing temperature is 180°C. The cutting time is 30min, and then transferred to a high-speed mixer for processing, the mixing speed is 1000r / min, and the mixing time is 30min to obtain modified asphalt;
[0038] (3) Preparation of bonding layer material: 100g of the above-mentioned modified asphalt is added in a high-speed mixer, and 5g of terpene resin, 10g of calcined kaolin, 5g ...
Embodiment 2
[0040] The difference between embodiment 2 and embodiment 1 is that the consumption of modifying agent is adjusted to 8g.
[0041] (1) Preparation of modifier: Add 0.05mol racemic polylactic acid, 0.055mol DCC and 0.055mol HOBt to tetrahydrofuran, heat to 55°C to dissolve, then add 0.06mol 3-(N-allylamino)propyl base trimethoxysilane, heated to 55 ° C for 8 hours, after the reaction, add water to precipitate, filter with suction, and dry to obtain the modifier;
[0042] (2) Preparation of modified asphalt: Heat 100g of 90# petroleum asphalt to 180°C to flow completely, then add 8g of the modifier prepared above, and transfer it to a high-speed shearing machine for processing, the shearing temperature is 180°C, and the shearing temperature is 180°C. The cutting time is 30min, and then transferred to a high-speed mixer for processing, the mixing speed is 1000r / min, and the mixing time is 30min to obtain modified asphalt;
[0043] (3) Preparation of bonding layer material: 100g ...
Embodiment 3
[0045] The difference between Example 2 and Example 1 is that the terpene resin is replaced by a modified terpene resin.
[0046] Preparation of modified terpene resin: Add 6.5g of β-pinene and 3.5g of vinylpyridine to toluene, add 0.5g of anhydrous aluminum chloride after dissolution, heat to 70°C for 5 hours, add water to terminate the reaction, Filtrate, wash the organic phase with water until neutral, and recover toluene by distillation under reduced pressure to obtain a modified terpene resin.
[0047](1) Preparation of modifier: Add 0.05mol racemic polylactic acid, 0.055mol DCC and 0.055mol HOBt to tetrahydrofuran, heat to 55°C to dissolve, then add 0.06mol 3-(N-allylamino)propyl base trimethoxysilane, heated to 55 ° C for 8 hours, after the reaction, add water to precipitate, filter with suction, and dry to obtain the modifier;
[0048] (2) Preparation of modified asphalt: heat 100g of 90# petroleum asphalt to 180°C to flow completely, then add 10g of the modifier prep...
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