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Preparation method of ultraviolet-excited red-light fluorescent powder for counterfeiting prevention

A technology of red fluorescent powder and mixed system, which is applied in the field of fluorescent powder, can solve the problems of not bright enough color, no anti-counterfeiting, and single function, and achieve the effects of preventing bleaching holes, bright colors, and long luminous efficacy

Inactive Publication Date: 2022-01-14
KUNMING UNIV OF SCI & TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] However, the phosphor powder prepared by the preparation method in the prior art has low intensity, insufficient color and single function, and does not have the function of anti-counterfeiting. Therefore, we propose a method for preparing an ultraviolet-excited red phosphor for anti-counterfeiting

Method used

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  • Preparation method of ultraviolet-excited red-light fluorescent powder for counterfeiting prevention
  • Preparation method of ultraviolet-excited red-light fluorescent powder for counterfeiting prevention
  • Preparation method of ultraviolet-excited red-light fluorescent powder for counterfeiting prevention

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Embodiment Construction

[0032] The present invention will be further explained below in conjunction with specific embodiments.

[0033] refer to figure 1 , embodiment one

[0034] In this example, a method for preparing an ultraviolet-excited red fluorescent powder for anti-counterfeiting is proposed, including the following raw materials: 62 parts of water, 12 parts of calcium salt, 22 parts of titanium oxide, 18 parts of europium oxide, barium sulfate 25 parts, 22 parts of magnesium sulfate, 3 parts of lithium phosphate, 3 parts of copper nitrate, 2 parts of activator, 4 parts of catalyst, 1 part of precipitant, 2 parts of complexing agent, the ratio of activator is phosphoric acid of 3:2:4 It is prepared by mixing propylenediamine, ammonium sulfate, ammonium chloride and ammonium hydroxide. The ratio of catalyst is 0.5:1:2. It is prepared by mixing active white mud, diatomaceous earth and saturated alkali solution. The ratio of precipitant is It is prepared by mixing dimethylglyoxime, ammonium b...

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Abstract

The invention discloses a preparation method of ultraviolet-excited red fluorescent powder for counterfeiting prevention. The method comprises the following raw materials in parts: 60-70 parts of water, 10-18 parts of calcium salt, 20-25 parts of titanium oxide, 15-26 parts of europium oxide, 20-35 parts of barium sulfate, 20-30 parts of magnesium sulfate, 1-5 parts of lithium phosphate, 1-5 parts of copper nitrate, 2-4 parts of activator, 4-8 parts of catalyst, 1-3 parts of precipitator and 2-6 parts of complexing agent. The activator is prepared by mixing propane diamine phosphate, ammonium sulfate, ammonium chloride and ammonium hydroxide according to the ratio of (3-6): (2-8): (4-6). The activator, the catalyst, the precipitator and the complexing agent are added in an existing preparation method, so that the prepared fluorescent powder is short in illumination but long in lighting effect, the preparation method is simple, the cost is low, the color is gorgeous; meanwhile, when a shielding object is placed at the position where the fluorescent powder is used, the shielded position becomes black, after the shielding object is taken off, the fluorescent powder can be recovered automatically, the fluorescent powder can be displayed by using other light, and the fluorescent powder can be used for instant anti-counterfeiting.

Description

technical field [0001] The invention relates to the technical field of fluorescent powder, in particular to a method for preparing an ultraviolet-excited red fluorescent powder for anti-counterfeiting. Background technique [0002] Phosphor powder, commonly known as luminous powder, is usually divided into two types: photo-induced energy storage luminous powder and radioactive luminous powder. Photo-energy storage luminous powder is a fluorescent powder that stores light energy after being irradiated by natural light, daylight, ultraviolet light, etc., and then slowly releases it in the form of fluorescence after stopping the light irradiation, so it can be used at night or in dark places. , can still see the luminescence, which lasts for several hours to more than ten hours. [0003] However, the phosphor powder prepared by the preparation method in the prior art has low intensity, not bright enough color and single function, and does not have the function of anti-counterf...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K11/62C09K11/78C09K11/81C09K11/84
CPCC09K11/7761C09K11/7731C09K11/7738C09K11/7741
Inventor 邱建备李锡正
Owner KUNMING UNIV OF SCI & TECH
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