Optical fiber and preparation method thereof
An optical fiber and fiber core technology, applied in the field of optical fiber and its preparation, can solve the problems of poor bending resistance, aggravating the fragility of the optical fiber, and fewer single-core fibers, so as to reduce the internal stress, improve the cross-linking density, and improve the bending resistance performance. Effect
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preparation example 1-7
[0039]The following is illustrated by taking Preparation Example 1 as an example, wherein the photoinitiator is (2,4,6-trimethylbenzoyl) diphenylphosphine oxide, and the CAS number is 75980-60-8; the solvent It is a mixture of diacetone alcohol (CAS No. 123-42-2), n-butyl acetate and propyl acetate, and the mass ratio of diacetone alcohol, n-butyl acetate and propyl acetate is 1:2:2; The grade of the six-functional aliphatic urethane acrylate is GN8601, purchased from Hunan Unico Chemical Technology Co., Ltd.; the grade of the hydroxyacrylate resin is FX-965, purchased from Nantong Fangxin Chemical Co., Ltd.; The oxyacrylate is bisphenol A epoxy acrylate, the grade is FX-8002-80, purchased from Fangxin Resin Technology Co., Ltd.; the additive is a mixture of Silok®355 silicone leveling agent and YWA-defoamer , the mass ratio of Silok®355 organic silicon leveling agent and YWA-defoamer is 2:1, and the Silok®355 organic silicon leveling agent is purchased from Shandong Moore Che...
preparation example 1
[0041] Preparation example 1 provides a kind of preparation method that contains the silicone rubber of UV curing coating, and its preparation steps are:
[0042] (1) Mix 0.06g photoinitiator and 2g solvent and stir evenly;
[0043] (2) Add 1.25g of hexafunctional aliphatic urethane acrylate, 2.5g of hydroxyacrylate resin and 1g of epoxy acrylate, and mix well;
[0044] (3) Add 0.003g additive, stir well, then add 3g solvent;
[0045] (4) Add 0.25 g of aliphatic urethane acrylate containing NCO groups before coating the surface with methyl vinyl phenyl silicone rubber to obtain a UV-curable coating;
[0046] (5) Coat the surface of 20 g of methyl vinyl phenyl silicone rubber with UV-curable coating to obtain silicone rubber containing UV-curable coating.
[0047] As shown in Table 1, the silicone rubbers containing UV-curable coatings of Preparation Examples 1-6 differ only in the quality of their raw materials.
[0048] Table 1
[0049] Preparation Example 1 ...
preparation example 8-11
[0050] Preparation Examples 8-11 are the same as Preparation Example 3, except that the raw materials for the preparation of silicone rubber containing UV-curable coatings are different:
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