Preparation method of auxiliary agent for improving compatibility of water reducing agent and retarder in cement mortar
A technology of cement mortar and water reducing agent, applied in the field of building materials, can solve the problems of early strength influence, reduced fluidity, shortened fluidity retention time, etc., so as to improve compatibility problems, increase fluidity, and maintain fluidity Performance-enhancing effects
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Embodiment 1
[0015] Provided is a preparation method of an auxiliary agent for improving the compatibility of a water reducing agent and a retarder in cement mortar, comprising the steps of:
[0016] (1) Using HPEG-2400 as the macromonomer and acrylic acid as the small monomer, the acid-ether ratio of the modified polyether and the acrylic acid is 4.5, based on the total mass of the modified polyether and acrylic acid, add the mass fraction 1% maleic anhydride and 1% vinyl phosphonic acid as comonomers, 0.4% hydrogen peroxide as initiator, 0.04% thioglycolic acid and 0.12 mass fraction The mercaptopropionic acid of % is transfer agent, and the vitamin C that massfraction is 0.05%% is reductant reaction synthesis and obtains auxiliary agent mother liquor;
[0017] (2) Remove water from the auxiliary agent mother liquor by vacuum distillation to obtain a high-purity water solution, then reduce the viscosity of the high-purity water solution mechanically to obtain a low-viscosity water soluti...
Embodiment 2
[0020] Provided is a preparation method of an auxiliary agent for improving the compatibility of a water reducing agent and a retarder in cement mortar, comprising the steps of:
[0021] (1) Using HPEG-2400 as the macromonomer and acrylic acid as the small monomer, the acid-ether ratio of the modified polyether and the acrylic acid is 5.0, based on the total mass of the modified polyether and acrylic acid, add the mass fraction 2% maleic anhydride and 2% vinyl phosphonic acid as comonomers, 0.6% hydrogen peroxide as initiator, 0.08% thioglycolic acid and 0.14 mass fraction % of mercaptopropionic acid is a transfer agent, and the vitamin C with a mass fraction of 0.5% is a reductant reaction synthesis to obtain an auxiliary agent mother liquor;
[0022] (2) Remove water from the auxiliary agent mother liquor by vacuum distillation to obtain a high-purity water solution, then reduce the viscosity of the high-purity water solution mechanically to obtain a low-viscosity water solu...
Embodiment 3
[0025] Provided is a preparation method of an auxiliary agent for improving the compatibility of a water reducing agent and a retarder in cement mortar, comprising the steps of:
[0026] (1) Using HPEG-2400 as the macromonomer and acrylic acid as the small monomer, the acid-ether ratio of the modified polyether and the acrylic acid is 4.5, based on the total mass of the modified polyether and acrylic acid, add the mass fraction 1.5% maleic anhydride and 1.5% vinyl phosphonic acid as comonomers, 0.5% hydrogen peroxide as initiator, 0.06% thioglycolic acid and 0.13% mass fraction Mercaptopropionic acid is a transfer agent, and vitamin C with a mass fraction of 0.3% is a reductant reaction synthesis to obtain an auxiliary agent mother liquor;
[0027] (2) Remove water from the auxiliary agent mother liquor by vacuum distillation to obtain a high-purity water solution, then reduce the viscosity of the high-purity water solution mechanically to obtain a low-viscosity water solution...
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