Supercritical extraction method of fruit and vegetable active substances

An active substance and supercritical technology, which is applied in solvent extraction, separation method, solid solvent extraction, etc., can solve the problems of increased flow rate, unfavorable extraction rate, and weakened extraction speed, so as to reduce the particle size of raw materials, increase the contact area, and extract The effect of speed increase

Active Publication Date: 2021-10-01
JIANGSU GAOKE PHARM EQUIP CO LTD
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Problems solved by technology

[0003] At present, during the supercritical extraction of active substances of fruits and vegetables, since the fruits and vegetables may contain pesticides, it is necessary to extract the pesticides together. The contact area between the solid and the solvent is small, so that the extraction speed is weakened. At the same time, most of the existing technologies are usually directly injected with CO 2 , while CO 2 If the flow rate is too large, it will cause CO in the extractor 2 As the flow rate increases, the CO 2 The residence time is shortened, and the contact time with the extract is reduced, which is not conducive to the improvement of the extraction rate. Also through this injection of CO 2 Pressurized situation, control CO 2 The flow rate may also cause the temperature and pressure in the extractor to not reach the required critical point, thereby reducing work efficiency

Method used

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  • Supercritical extraction method of fruit and vegetable active substances
  • Supercritical extraction method of fruit and vegetable active substances
  • Supercritical extraction method of fruit and vegetable active substances

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Embodiment

[0036] A method for supercritical extraction of fruit and vegetable active substances, comprising the following steps:

[0037] S1. During the supercritical extraction process of fruit and vegetable active substances, the extraction needs to be carried out at close to room temperature (35-40°C);

[0038] S2, placing the fruit and vegetable active substances in the extraction device, fixing the pressure value in the extraction device by adjusting, and separating the pesticides by changing the temperature;

[0039] S3. The temperature value is fixed again, and the vegetable active substances are separated by reducing the pressure, so as to complete the extraction of the whole fruit and vegetable active substances.

[0040] see Figure 1-6 , the extraction device in S2 includes a storage tank 1, an extractor 2 is provided on the right side of the storage tank 1, an electric heater 3 is provided outside the extractor 2, a pressurizer 4 is provided on the right side of the storage...

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Abstract

The invention discloses a supercritical extraction method of fruit and vegetable active substances, and belongs to the technical field of supercritical extraction. When the device needs to perform supercritical extraction of fruit and vegetable active substances, an electric heater and a pressurizer are started to heat and apply pressure to an extractor, a deformation air bag deforms due to pressure, magnetic insulation powder originally making contact with one another in an inner cavity is gradually separated, a magnet block emits magnetism to the outside, a plurality of separating rotating beads between the inner walls of a groove are affected by an annular magnetic field to do circular motion and rotate all the time, fruits and vegetables placed inside are decomposed and fall into screening holes, and preliminary screening is conducted. Due to the fact that the granularity of raw materials is reduced, the contact area of solids and a solvent is increased, the extraction speed is increased, the screened raw material particles cannot be too small or too fine, the situation that too small or too fine particles block sieve holes is avoided, and therefore, blockage of a filter screen at an outlet of the extractor is avoided, and working efficiency is improved.

Description

technical field [0001] The invention relates to the technical field of supercritical extraction, in particular to a supercritical extraction method of fruit and vegetable active substances. Background technique [0002] Supercritical is a supercritical fluid, which is a state of matter that is neither gaseous nor liquid between gas and liquid. This substance can only exist when its temperature and pressure exceed the critical point. The density of supercritical fluid is relatively high. Large, similar to liquid, and its viscosity is closer to gas, so supercritical fluid is a very ideal extraction agent. [0003] At present, during the supercritical extraction of active substances of fruits and vegetables, since the fruits and vegetables may contain pesticides, it is necessary to extract the pesticides together. The contact area between the solid and the solvent is small, so that the extraction speed is weakened. At the same time, most of the existing technologies are usuall...

Claims

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Application Information

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IPC IPC(8): B01D11/02B02C19/00B02C23/08
CPCB01D11/0203B01D11/0207B02C19/0056B02C23/08
Inventor 沈立华吴进富
Owner JIANGSU GAOKE PHARM EQUIP CO LTD
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