Siraitia grosvenorii sugar with improved sweetness and preparation method thereof
A technology of Monk fruit candy and Monk fruit, applied in food ingredients as taste improver, food drying, food science and other directions, can solve problems such as poor taste and taste performance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example 1
[0061] Preparation example 1 Cross-linking modification of XDA-200B resin
[0062] Add 1kg of XDA-200B resin, 3.5L of BCMB, and 12L of carbon tetrachloride into a stirred reactor, let it swell for 10 hours, add 0.2kg of anhydrous zinc chloride, and react at 60°C for 12 hours, After the reaction, wash with absolute ethanol and deionized water until no precipitation occurs after adding the nitrate solution to obtain chloromethylated XDA-200B resin. Chloromethylated XDA-200B resin was added to 12L dimethyl sulfoxide after water removal to swell for 8h, and slowly added 0.2kg anhydrous aluminum chloride, 0.1kg anhydrous zinc chloride and 0.08kg triethylenetetramine , heated to 50°C and reacted for 12 hours under stirring conditions, filtered, washed with absolute ethanol and deionized water respectively, until no precipitation occurred after adding the nitrate solution, put the obtained resin in a blower dryer, and vacuum-dried overnight at 60°C, A cross-linked modified XDA-200B ...
preparation example 2
[0064] Preparation example 2 Cross-linking modification of LSA-5B resin
[0065] Add 1kg of LSA-5B resin, 3.5L of BCMB, and 12L of carbon tetrachloride into a stirred reactor, let it swell for 10 hours, add 0.2kg of anhydrous zinc chloride, and react at 60°C for 12 hours, After the reaction, wash with absolute ethanol and deionized water until no precipitation occurs after adding the nitrate solution to obtain chloromethylated LSA-5B resin. Chloromethylated LSA-5B resin was added to 12L dimethyl sulfoxide after dehydration to swell for 8h, slowly added 0.2kg anhydrous aluminum chloride, 0.1kg anhydrous zinc chloride and 0.12k ethylenediamine, and heated React at 50°C for 12h under stirring conditions, filter, wash with absolute ethanol and deionized water respectively, until no precipitation occurs after adding the nitrate solution, place the obtained resin in a blower dryer, and vacuum dry overnight at 60°C to obtain cross-linked Co-modified LSA-5B resin.
[0066] After tes...
Embodiment 1
[0068] (1) 80 kg of LX-17 resin is preliminarily packed in a stainless steel chromatography column and treated with ethanol, 4% aqueous sodium hydroxide solution, and 4% hydrochloric acid according to the standard procedure for regeneration of macroporous adsorption resin for use. Take 10kg of mogroside V50 powder, add 150L of purified water, stir to dissolve, then pass the solution through a chromatography column equipped with LX-17 resin, and collect the feed effluent; after feeding the material, add 130L of purified water to wash the resin column , collect the washing solution, and combine the feed effluent and the washing solution.
[0069] (2) 18kg of cross-linked modified XDA-200B resin obtained in preparation example 1 in advance in the stainless steel chromatographic column and treated with ethanol, 4% sodium hydroxide aqueous solution, 4% hydrochloric acid according to the standard procedure of macroporous adsorption resin regeneration treatment use. Pass the combine...
PUM
Property | Measurement | Unit |
---|---|---|
Particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com