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Siraitia grosvenorii sugar with improved sweetness and preparation method thereof

A technology of Monk fruit candy and Monk fruit, applied in food ingredients as taste improver, food drying, food science and other directions, can solve problems such as poor taste and taste performance

Pending Publication Date: 2021-07-06
HUNAN HUACHENG BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0012] In order to solve the defects of poor taste and taste properties of mogroside-based sweeteners in the prior art, the present invention proposes a method that utilizes the most common mogroside V50 on the market as a raw material and passes through a polar macroporous adsorption resin column. , high specific surface activity macroporous adsorption resin column, small pore reversed-phase gel column, activated carbon chromatography, and then add sucrose / brown sugar and arabinose for compounding, and finally prepare a kind of low sweetness (sweetness is sucrose / brown sugar 1-15 times), the taste is close to sucrose's monk fruit sugar

Method used

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  • Siraitia grosvenorii sugar with improved sweetness and preparation method thereof

Examples

Experimental program
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Effect test

preparation example 1

[0061] Preparation example 1 Cross-linking modification of XDA-200B resin

[0062] Add 1kg of XDA-200B resin, 3.5L of BCMB, and 12L of carbon tetrachloride into a stirred reactor, let it swell for 10 hours, add 0.2kg of anhydrous zinc chloride, and react at 60°C for 12 hours, After the reaction, wash with absolute ethanol and deionized water until no precipitation occurs after adding the nitrate solution to obtain chloromethylated XDA-200B resin. Chloromethylated XDA-200B resin was added to 12L dimethyl sulfoxide after water removal to swell for 8h, and slowly added 0.2kg anhydrous aluminum chloride, 0.1kg anhydrous zinc chloride and 0.08kg triethylenetetramine , heated to 50°C and reacted for 12 hours under stirring conditions, filtered, washed with absolute ethanol and deionized water respectively, until no precipitation occurred after adding the nitrate solution, put the obtained resin in a blower dryer, and vacuum-dried overnight at 60°C, A cross-linked modified XDA-200B ...

preparation example 2

[0064] Preparation example 2 Cross-linking modification of LSA-5B resin

[0065] Add 1kg of LSA-5B resin, 3.5L of BCMB, and 12L of carbon tetrachloride into a stirred reactor, let it swell for 10 hours, add 0.2kg of anhydrous zinc chloride, and react at 60°C for 12 hours, After the reaction, wash with absolute ethanol and deionized water until no precipitation occurs after adding the nitrate solution to obtain chloromethylated LSA-5B resin. Chloromethylated LSA-5B resin was added to 12L dimethyl sulfoxide after dehydration to swell for 8h, slowly added 0.2kg anhydrous aluminum chloride, 0.1kg anhydrous zinc chloride and 0.12k ethylenediamine, and heated React at 50°C for 12h under stirring conditions, filter, wash with absolute ethanol and deionized water respectively, until no precipitation occurs after adding the nitrate solution, place the obtained resin in a blower dryer, and vacuum dry overnight at 60°C to obtain cross-linked Co-modified LSA-5B resin.

[0066] After tes...

Embodiment 1

[0068] (1) 80 kg of LX-17 resin is preliminarily packed in a stainless steel chromatography column and treated with ethanol, 4% aqueous sodium hydroxide solution, and 4% hydrochloric acid according to the standard procedure for regeneration of macroporous adsorption resin for use. Take 10kg of mogroside V50 powder, add 150L of purified water, stir to dissolve, then pass the solution through a chromatography column equipped with LX-17 resin, and collect the feed effluent; after feeding the material, add 130L of purified water to wash the resin column , collect the washing solution, and combine the feed effluent and the washing solution.

[0069] (2) 18kg of cross-linked modified XDA-200B resin obtained in preparation example 1 in advance in the stainless steel chromatographic column and treated with ethanol, 4% sodium hydroxide aqueous solution, 4% hydrochloric acid according to the standard procedure of macroporous adsorption resin regeneration treatment use. Pass the combine...

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Abstract

The invention relates to siraitia grosvenorii sugar with improved sweetness and a preparation method of the siraitia grosvenorii sugar. The siraitia grosvenorii sugar comprises the following ingredients in percentage by mass: 0.1 to 2.1 wt precent of mogroside V, 0.02 to 0.40 wt precent of other triterpene glucosides, 10 to 50 wt percent of cane sugar / brown sugar and 48 to 89 wt percent of arabinose. The siraitia grosvenorii sugar is prepared by compounding siraitia grosvenorii high-power sweetening agent, cane sugar / brown sugar and arabinose; the siraitia grosvenorii high-power sweetening agent is prepared from mogroside as a raw material treated through sequentially passing through a polar macroporous adsorption resin column, a high-specific-surface-activity macroporous adsorption resin column and a small-hole reversed-phase gel column for physically refining; and the siraitia grosvenorii high-power sweetening agent is prepared from the following ingredients of 55 to 70 wt percent of mogroside V, 1.5 to 4 wt percent of mogroside IV, 3 to 10 wt percent of 11-O-mogroside V, 0.5 to 1.8 wt percent of siamenoside, 0.4 to 1.5 wt percent of mogroside VI, less than 0.2 wt percent of acid phenolic substances and less than 0.2 wt percent of pigment substances. According to a mogroside sugar substitute, the sweetness multiple is reduced, the sweet lasting time is shortened, the preparation taste is excellent, and the siraitia grosvenorii sugar is a sweet substitute easy to be accepted by consumers.

Description

technical field [0001] The invention relates to the technical field of plant extraction and separation and the field of sweetener compounding, in particular to a monk fructose with improved sweetness performance and a preparation method thereof. Background technique [0002] Mogroside is prepared from the fresh ripe fruit of Luo Han Guo, a plant of Cucurbitaceae, which is saccharified and then ripened, and then prepared through a series of separation and extraction steps. Among them, the most common commercially available mogroside is the V50 specification, and the content of mogroside V is around 50%. The main process is to prepare fresh Luo Han Guo through saccharification, ripening, crushing, water extraction, filtration, ceramic membrane microfiltration clarification, broad-spectrum macroporous adsorption resin chromatography, ion exchange resin decolorization, desalination, vacuum concentration, spray drying and other steps. have to. Mogroside has the best taste among...

Claims

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Application Information

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IPC IPC(8): A23L27/30A23L5/20
CPCA23L27/36A23L27/38A23L27/33A23L5/273A23V2002/00A23V2200/16A23V2250/254A23V2250/628A23V2250/602A23V2300/10
Inventor 刘庚贵曾润清黄华学黄俊何安乐
Owner HUNAN HUACHENG BIOTECH
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