High-water-content oil sludge reconstruction method
A water-oil and oil-sludge technology, applied in chemical instruments and methods, water/sludge/sewage treatment, dehydration/drying/concentrated sludge treatment, etc., can solve equipment maintenance costs, depreciation costs and high treatment costs, and easy equipment Problems such as coking and blockage, flammability and explosion, etc., achieve the effect of significant resource utilization, small investment, and low safety risk
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Embodiment 1
[0047] The sample treated in this example is high water content oil sludge (moisture content 88.74%, oil content 7.79%, solid content 3.47%) of a petrochemical plant in Lanzhou
[0048] In this example S1, weigh 300 g of the above-mentioned high-water-containing oil sludge and 135 g of special phase-transfer agent into a 1000 ml flask with stirring, raise the temperature to 50 ° C, and stir at a speed of 80 rpm for 10 minutes to obtain an evenly mixed water-containing oil sludge in an unstable state Pickering-like emulsion system;
[0049] In this example S2, 435 g of the unsteady high-water-containing oily sludge Pickering emulsion system obtained by uniform mixing containing a phase transfer agent prepared in S1 was put into a homogenizer and homogenized for 5 minutes at a temperature of 50 ° C and a shear rate of 5000 rpm. , to obtain an unsteady homogeneous oil-based suspended solids system; after centrifugation, 184.2 g of oil sludge was obtained.
[0050] The oil sludge o...
Embodiment 2
[0053] The sample treated in this example is a high water content oil sludge (water content 68.58%, oil content 16.81%, solid content 14.61%) of a petrochemical plant in Jiujiang
[0054] In this example S1, weigh 300g of the above-mentioned high-water-content sludge and 135g of special phase-transfer agent into a 1000ml flask with stirring, raise the temperature to 50°C, and stir for 10 minutes at a rotation speed of 80rpm to obtain an unsteady high-water-content mixture evenly mixed. Oil sludge Pickering emulsion system;
[0055] In this example S2, 435 g of the unsteady high-water-containing oily sludge Pickering emulsion system obtained by uniform mixing containing a phase transfer agent prepared in S1 was put into a homogenizer and homogenized for 3 minutes at a temperature of 50 ° C and a shear rate of 8000 rpm. , to obtain an unsteady homogeneous oil-based suspended solids system; after centrifugation, 217.8 g of oil sludge was obtained.
[0056] The oil sludge obtaine...
Embodiment 3
[0058] Embodiment 3: The sample treated in this embodiment is a high water content oil sludge (water content 68.58%, oil content 16.81%, solid content 14.61%) of a petrochemical plant in Jiujiang
[0059] In this example S1, weigh 300g of the above-mentioned high-water-content sludge and 135g of special phase-transfer agent into a 1000ml flask with stirring, raise the temperature to 50°C, and stir for 10 minutes at a rotation speed of 80rpm to obtain an unsteady high-water-content mixture evenly mixed. Oil sludge Pickering emulsion system;
[0060] In this example S2, 435 g of the unsteady high-water-containing oily sludge Pickering emulsion system obtained by uniform mixing containing a phase transfer agent prepared in S1 was put into a homogenizer and homogenized for 5 minutes at a temperature of 50 ° C and a shear rate of 5000 rpm. , to obtain an unsteady homogeneous oil-based suspended matter system; after centrifugation, 221g of oil sludge was obtained.
[0061] The oil ...
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