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A kind of hard hydrophobic coating with micro-nano structure and preparation method thereof

A technology of micro-nano structure and hydrophobic coating, applied in coating, metal material coating process, vacuum evaporation plating, etc., can solve the problems of easy aging and poor wear resistance of hydrophobic coating, reduce surface wear, improve Effects of hardness and wear resistance, good friction-reducing and self-lubricating properties

Active Publication Date: 2022-05-13
宁波云涂科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to overcome the shortcomings of poor wear resistance and easy aging of hydrophobic coatings, and provide a hard hydrophobic coating with micro-nano structure and its preparation method

Method used

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  • A kind of hard hydrophobic coating with micro-nano structure and preparation method thereof
  • A kind of hard hydrophobic coating with micro-nano structure and preparation method thereof
  • A kind of hard hydrophobic coating with micro-nano structure and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] The 3×3cm high-speed steel sample block is used as the base material, and the specific implementation steps are as follows:

[0040] 1) Clean the surface of the high-speed steel substrate with acetone, alcohol and deionized water in sequence, and dry it with a hair dryer;

[0041]2) Deposit the Cr layer first by using multi-arc ion plating to deposit the coating:

[0042] The working air pressure is 0.4Pa, the substrate bias voltage is -450V, the substrate temperature is 550℃, and the deposition time of Cr target alone is 10min;

[0043] Then deposit the CrTiAlN layer:

[0044] The working pressure is 2Pa, the substrate bias is -60V, and the Cr target and the TiAl target are co-sputtered for 120min under the condition that the flow ratio of argon and nitrogen is 1:9.

[0045] Finally deposit the CrTiAlCN layer:

[0046] The working pressure is 2Pa, the substrate bias is -60V, the Cr target and the TiAl target are co-sputtered under the condition that the flow ratio o...

Embodiment 2

[0049] The 5×5cm P20 mold steel sample block is used as the base material, and the specific implementation steps are as follows:

[0050] 1) Clean the surface of the P20 steel substrate with acetone, alcohol and deionized water in sequence, and dry it with a hair dryer;

[0051] 2) Deposit the Cr layer first:

[0052] The working air pressure is 0.3Pa, the substrate bias voltage is -350V, the substrate temperature is 280℃, and the deposition time of Cr target alone is 10min;

[0053] Then deposit the CrTiAlN layer:

[0054] The working pressure is 2.2Pa, the substrate bias is -60V, and the Cr target and TiAl target are co-sputtered for 120min under the condition that the flow ratio of argon and nitrogen is 1:15;

[0055] Finally deposit the CrTiAlCN layer:

[0056] The working pressure is 2.2Pa, the substrate bias is -60V, the Cr target and the TiAl target are co-sputtered under the condition that the flow ratio of argon and nitrogen is 1:15, and a carbon ion beam with an e...

Embodiment 3

[0059] The 3×3cm H13 mold steel sample block is used as the base material, and the specific implementation steps are as follows:

[0060] 1) First clean the surface of the H13 steel substrate with acetone, alcohol and deionized water in sequence, and dry it with a hair dryer;

[0061] 2) Deposit the Cr layer first:

[0062] The working air pressure is 0.3Pa, the substrate bias voltage is -350V, the substrate temperature is 450℃, and the deposition time of Cr target alone is 10min;

[0063] Then deposit the CrTiAlN layer:

[0064] The working pressure is 2.2Pa, the substrate bias is -80V, and the Cr target and the TiAl target are co-sputtered for 120min under the condition that the flow ratio of argon and nitrogen is 1:20.

[0065] Finally deposit the CrTiAlCN layer:

[0066] The working pressure is 2.2Pa, the substrate bias is -80V, the Cr target and the TiAl target are co-sputtered under the condition that the flow ratio of argon and nitrogen is 1:20, and a carbon ion beam...

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Abstract

The invention discloses a hard hydrophobic coating with a micro-nano structure and a preparation method thereof, and relates to the field of hydrophobic coatings. In the preparation method of the present invention, the Cr layer and the CrTiAlN layer are sequentially deposited using a multi-arc ion plating equipment with an ion beam auxiliary device, and then irradiated with a medium-energy carbon ion beam, and carbon ions are also implanted into the CrTiAlN layer during etching. , the formed CrTiAlCN metal carbide has a higher hardness than its nitride, which further improves the hardness and wear resistance of the entire coating; the CrTiAlCN obtained after the medium-energy carbon ion beam treatment retains the CrTiAlN film hard On the basis of quality and wear resistance, its hydrophobicity is further improved; carbon also has good friction-reducing and self-lubricating properties, which can reduce coating surface wear and polymer material adhesion; the preparation method of the present invention has simple process and can be directly applied Produced on a large scale in industry.

Description

technical field [0001] The invention relates to the field of hydrophobic coatings, in particular to a hard hydrophobic coating with a micro-nano structure and a preparation method thereof. Background technique [0002] It is the most commonly used method in the industry to produce plastic, rubber and other polymer material parts with specific shapes through mold injection molding, which has a huge production scale and is widely used. One of the biggest difficulties in its production process is to solve the adhesion problem between the molded part and the mold, that is, to enhance the release property of the mold. Generally, the method commonly used in industry to enhance the release performance of molds is to use release agents, but release agents have disadvantages such as high price, great harm to human body, and corrosive effect on molds, which are uneconomical and not environmentally friendly. There is an urgent need for better alternative technologies. By preparing a ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/06C23C14/16C23C14/32C23C14/58B29C33/56
CPCC23C14/0664C23C14/0641C23C14/16C23C14/325C23C14/0021C23C14/5873B29C33/56
Inventor 张星翔马洋张颖
Owner 宁波云涂科技有限公司
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