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Preparation method of rose essential oil and the rose essential oil

A technology of rose essential oil and rose petals, which is applied in the directions of essential oils/spices and fat production, can solve the problems of destroying essential oil components, low purity of essential oil products, and low extraction rate of essential oils, avoiding damage, ensuring extraction efficiency and product quality. quality effect

Pending Publication Date: 2020-11-10
玉溪擎禹农业科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the extraction rate of essential oil by steam distillation is low, and the temperature of the extraction process is too high, which will destroy some components in the essential oil, so that the purity of the formed essential oil product is not high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Present embodiment provides a kind of preparation method of rose essential oil, comprises the steps:

[0043] S1, preprocessing; specifically includes the following steps:

[0044] S11, picking and cleaning: wash the picked rose petals with clean water and drain them for later use;

[0045] S12, freezing treatment: weighing a certain amount of rose petals obtained in step S11, and freezing at a temperature of -15°C for 1.5 hours;

[0046] S13, add water to defrost: add deionized water to the frozen rose petals obtained in step S12, and slowly melt at a temperature of 80°C to 100°C until the rose petals are softened, wherein the amount of deionized water added meets the ratio of solid to liquid It is 4:1.

[0047] S2, distillation; specifically include the following steps:

[0048] S21, distillation operation: transfer the solid-liquid mixture after the pretreatment to a still, the distillation temperature is 180° C., the distillation time is 2.0 h, and an oil-water m...

Embodiment 2

[0052] Present embodiment provides a kind of preparation method of rose essential oil, comprises the steps:

[0053] S1, preprocessing; specifically includes the following steps:

[0054] S11, picking and cleaning: wash the picked rose petals with clean water and drain them for later use;

[0055] S12, freezing treatment: weighing a certain amount of rose petals obtained in step S11, and freezing at a temperature of -15°C for 1.5 hours;

[0056] S13, add water to defrost: add deionized water to the frozen rose petals obtained in step S12, and slowly melt at a temperature of 80°C to 100°C until the rose petals are softened, wherein the amount of deionized water added meets the ratio of solid to liquid is 4:1;

[0057] S14, crushing and homogenizing: the thawed rose petals in step S13 were crushed at a speed of 800 r / min for 5 minutes to prepare a homogeneous slurry.

[0058] S2, distillation; specifically include the following steps:

[0059] S21, distillation operation: tr...

Embodiment 3

[0063] Present embodiment provides a kind of preparation method of rose essential oil, comprises the steps:

[0064] S1, preprocessing; specifically includes the following steps:

[0065] S11, picking and cleaning: wash the picked rose petals with clean water and drain them for later use;

[0066] S12, freezing treatment: weighing a certain amount of rose petals obtained in step S11, and freezing at a temperature of -15°C for 1.5 hours;

[0067] S13, add water to defrost: add deionized water to the frozen rose petals obtained in step S12, and slowly melt at a temperature of 80°C to 100°C until the rose petals are softened, wherein the amount of deionized water added meets the ratio of solid to liquid is 4:1;

[0068] S14, crushing and homogenizing: crushing the thawed rose petals in step S13 at a speed of 800 r / min for 5 minutes to prepare a uniform slurry;

[0069] S15, ultrasonic treatment: the homogeneous slurry obtained in step S14 was ultrasonically treated at 50° C. f...

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PUM

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Abstract

The invention provides a preparation method of rose essential oil. The preparation method comprises a pretreatment step and a distillation step, wherein the pretreatment step comprises the following specific steps: S11, picking and cleaning: cleaning picked rose petals with clear water, and draining for later use; s12, freezing treatment: freezing the rose petals obtained in the step S11 at the temperature of -25 to -5 DEG C for 1-3 hours; and S13, defrozing with water: adding deionized water into the frozen rose petals obtained in the step S12, and slowly melting the ice at the temperature of80-100 DEG C until the rose petals are softened, wherein the adding amount of the deionized water meets the condition that the material-liquid ratio is (3-6):1. The preparation method disclosed by the invention has the advantages of higher essential oil extraction rate and higher essential oil extraction efficiency, and can be used for obtaining high-purity and non-destructive rose essential oil.The invention also provides the rose essential oil prepared by the preparation method.

Description

technical field [0001] The invention belongs to the technical field of extraction of plant active components, and in particular relates to a preparation method of rose essential oil and rose essential oil. Background technique [0002] With the development of society and the improvement of people's living standards, rose essential oil, known as "liquid gold", has been favored by more and more people. Rose essential oil has great benefits for human health. Metabolism function, and rose essential oil also has very good effect on aging skin at the same time, so rose essential oil is widely used in fields such as skin care products, medicine, has huge economic value and practical value. [0003] Rose essential oil is extracted from natural roses. The existing extraction methods of rose essential oil mainly include pressing method, steam distillation method, solvent extraction method, supercritical fluid / subcritical fluid method, molecular distillation and other methods. Among t...

Claims

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Application Information

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IPC IPC(8): C11B9/02
CPCC11B9/02C11B9/027
Inventor 左帅
Owner 玉溪擎禹农业科技有限公司
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